ChemicalBook > CAS DataBase List > 3-IODO-4-METHOXY-BENZALDEHYDE

3-IODO-4-METHOXY-BENZALDEHYDE

Product Name
3-IODO-4-METHOXY-BENZALDEHYDE
CAS No.
2314-37-6
Chemical Name
3-IODO-4-METHOXY-BENZALDEHYDE
Synonyms
3-IODO-4-METHOXY-BENZALDEHYDE;Benzaldehyde, 3-iodo-4-methoxy-;3-Iodo-4-methoxybenzaldehyde 97%;3-Iodo-p-anisaldehyde, 4-Formyl-2-iodoanisole
CBNumber
CB6736086
Molecular Formula
C8H7IO2
Formula Weight
262.04
MOL File
2314-37-6.mol
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3-IODO-4-METHOXY-BENZALDEHYDE Property

Melting point:
107-112℃
Boiling point:
325.0±32.0 °C(Predicted)
Density 
1.780±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
form 
Solid
color 
White to off-white/yellow
Sensitive 
Air & Light Sensitive
InChI
InChI=1S/C8H7IO2/c1-11-8-3-2-6(5-10)4-7(8)9/h2-5H,1H3
InChIKey
RVWOHBWQJGLXIJ-UHFFFAOYSA-N
SMILES
C(=O)C1=CC=C(OC)C(I)=C1
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Safety

Hazard Codes 
Xn,N
Risk Statements 
22-50
Safety Statements 
61
RIDADR 
UN 2811 6.1 / PGIII
WGK Germany 
3
HazardClass 
6.1
HS Code 
2912290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

H400Very toxic to aquatic life

Precautionary statements

P273Avoid release to the environment.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
722278
Product name
3-Iodo-4-methoxybenzaldehyde
Purity
97%
Packaging
1g
Price
$26.95
Updated
2025/07/31
TRC
Product number
I708663
Product name
3-Iodo-4-methoxybenzaldehyde
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
I708663
Product name
3-Iodo-4-methoxybenzaldehyde
Packaging
50mg
Price
$45
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0021969
Product name
3-IODO-4-METHOXY-BENZALDEHYDE
Purity
95.00%
Packaging
1G
Price
$1280.66
Updated
2021/12/16
AK Scientific
Product number
5347AH
Product name
3-Iodo-4-methoxy-benzaldehyde
Packaging
5g
Price
$266
Updated
2021/12/16
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3-IODO-4-METHOXY-BENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

123-11-5

2314-37-6

General procedure for the synthesis of compounds (CAS:2314-37-6) from p-methoxybenzaldehyde: To a solution (0.1 M) of dichloromethane (CH2Cl2) or 1,2-dichloroethane ((CH2Cl)2) in stirring (1 mmol) of the substrate (1 mmol), Ph3PAuNTf2 (0.025 mmol, 19 mg; if using the 2:1 complex of Ph3PAuNTf2 with toluene), followed by N-iodosuccinimide (1.1 mmol, 248 mg). The reaction mixture was stirred at room temperature or reacted under reflux conditions until complete conversion of the feedstock. Upon completion of the reaction, the solvent was removed under reduced pressure and the crude product was purified by fast column chromatography using different ratios of hexane and ethyl acetate (EtOAc) as eluents to give the final pure target product.

References

[1] European Journal of Organic Chemistry, 2000, # 8, p. 1527 - 1533
[2] European Journal of Organic Chemistry, 2012, # 30, p. 5935 - 5942,8
[3] Synthesis, 2010, # 16, p. 2776 - 2786
[4] Organic letters, 2003, vol. 5, # 4, p. 415 - 418
[5] Tetrahedron Letters, 1997, vol. 38, # 35, p. 6305 - 6306

3-IODO-4-METHOXY-BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-IODO-4-METHOXY-BENZALDEHYDE Suppliers

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View Lastest Price from 3-IODO-4-METHOXY-BENZALDEHYDE manufacturers

Career Henan Chemical Co
Product
3-iodo-4-methoxybenzaldehyde 2314-37-6
Price
US $0.10/g
Min. Order
1g
Purity
98%min
Supply Ability
10g,100g,1kg
Release date
2020-01-09

2314-37-6, 3-IODO-4-METHOXY-BENZALDEHYDERelated Search:


  • 3-IODO-4-METHOXY-BENZALDEHYDE
  • 3-Iodo-p-anisaldehyde, 4-Formyl-2-iodoanisole
  • 3-Iodo-4-methoxybenzaldehyde 97%
  • Benzaldehyde, 3-iodo-4-methoxy-
  • 2314-37-6
  • aldehyde| alkyl Iodine
  • Adehydes, Acetals & Ketones
  • Anisoles, Alkyloxy Compounds & Phenylacetates
  • Iodine Compounds