3-IODO-4-METHOXY-BENZALDEHYDE
- Product Name
- 3-IODO-4-METHOXY-BENZALDEHYDE
- CAS No.
- 2314-37-6
- Chemical Name
- 3-IODO-4-METHOXY-BENZALDEHYDE
- Synonyms
- 3-IODO-4-METHOXY-BENZALDEHYDE;Benzaldehyde, 3-iodo-4-methoxy-;3-Iodo-4-methoxybenzaldehyde 97%;3-Iodo-p-anisaldehyde, 4-Formyl-2-iodoanisole
- CBNumber
- CB6736086
- Molecular Formula
- C8H7IO2
- Formula Weight
- 262.04
- MOL File
- 2314-37-6.mol
3-IODO-4-METHOXY-BENZALDEHYDE Property
- Melting point:
- 107-112℃
- Boiling point:
- 325.0±32.0 °C(Predicted)
- Density
- 1.780±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- form
- Solid
- color
- White to off-white/yellow
- Sensitive
- Air & Light Sensitive
- InChI
- InChI=1S/C8H7IO2/c1-11-8-3-2-6(5-10)4-7(8)9/h2-5H,1H3
- InChIKey
- RVWOHBWQJGLXIJ-UHFFFAOYSA-N
- SMILES
- C(=O)C1=CC=C(OC)C(I)=C1
N-Bromosuccinimide Price
- Product number
- 722278
- Product name
- 3-Iodo-4-methoxybenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $26.95
- Updated
- 2025/07/31
- Product number
- I708663
- Product name
- 3-Iodo-4-methoxybenzaldehyde
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- I708663
- Product name
- 3-Iodo-4-methoxybenzaldehyde
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- HCH0021969
- Product name
- 3-IODO-4-METHOXY-BENZALDEHYDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1280.66
- Updated
- 2021/12/16
- Product number
- 5347AH
- Product name
- 3-Iodo-4-methoxy-benzaldehyde
- Packaging
- 5g
- Price
- $266
- Updated
- 2021/12/16
3-IODO-4-METHOXY-BENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
123-11-5
2314-37-6
General procedure for the synthesis of compounds (CAS:2314-37-6) from p-methoxybenzaldehyde: To a solution (0.1 M) of dichloromethane (CH2Cl2) or 1,2-dichloroethane ((CH2Cl)2) in stirring (1 mmol) of the substrate (1 mmol), Ph3PAuNTf2 (0.025 mmol, 19 mg; if using the 2:1 complex of Ph3PAuNTf2 with toluene), followed by N-iodosuccinimide (1.1 mmol, 248 mg). The reaction mixture was stirred at room temperature or reacted under reflux conditions until complete conversion of the feedstock. Upon completion of the reaction, the solvent was removed under reduced pressure and the crude product was purified by fast column chromatography using different ratios of hexane and ethyl acetate (EtOAc) as eluents to give the final pure target product.
References
[1] European Journal of Organic Chemistry, 2000, # 8, p. 1527 - 1533
[2] European Journal of Organic Chemistry, 2012, # 30, p. 5935 - 5942,8
[3] Synthesis, 2010, # 16, p. 2776 - 2786
[4] Organic letters, 2003, vol. 5, # 4, p. 415 - 418
[5] Tetrahedron Letters, 1997, vol. 38, # 35, p. 6305 - 6306
3-IODO-4-METHOXY-BENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-IODO-4-METHOXY-BENZALDEHYDE Suppliers
- Tel
- --
- Fax
- --
- contact@achemica.com
- Country
- Switzerland
- ProdList
- 6155
- Advantage
- 50
View Lastest Price from 3-IODO-4-METHOXY-BENZALDEHYDE manufacturers
- Product
- 3-iodo-4-methoxybenzaldehyde 2314-37-6
- Price
- US $0.10/g
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- 10g,100g,1kg
- Release date
- 2020-01-09