ChemicalBook > CAS DataBase List > 2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE

2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE

Product Name
2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE
CAS No.
1007-99-4
Chemical Name
2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE
Synonyms
2-Amino-6-chloro-5-nitropyrimidin-4-ol;ACHNP;AKOS 92816;2-Amino-6-chloro-5-nitro-4(3H)-pyrimidone;2-amino-6-chloro-5-nitro-1H-pyrimidin-4-one;2-Amino-6-chloro-5-nitropyrimidin-4(5H)-one;2-Amino-6-chloro-5-nitro-4(1H)-pyrimidinone;2-azanyl-6-chloro-5-nitro-1H-pyrimidin-4-one;4(1H)-Pyrimidinone,2-amino-6-chloro-5-nitro-;2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE
CBNumber
CB6747046
Molecular Formula
C4H3ClN4O3
Formula Weight
190.54
MOL File
1007-99-4.mol
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2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE Property

storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
Boiling point:
268.2±50.0 °C(Predicted)
Density 
2.20±0.1 g/cm3(Predicted)
Melting point:
>350 °C
pka
4≅+-.0.50(Predicted)
CAS DataBase Reference
1007-99-4(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A604163
Product name
2-Amino-4-chloro-6-hydroxy-5-nitropyrimidine
Packaging
50mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-W000783
Product name
2-amino-6-chloro-5-nitropyrimidin-4-ol
Packaging
100mg
Price
$58
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA12037
Product name
2-Amino-4-chloro-5-nitro-6-hydroxypyrimidine
Packaging
500mg
Price
$200
Updated
2021/12/16
Matrix Scientific
Product number
094520
Product name
2-Amino-4-chloro-6-hydroxy-5-nitropyrimidine
Purity
95+%
Packaging
1g
Price
$265
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA12037
Product name
2-Amino-4-chloro-5-nitro-6-hydroxypyrimidine
Packaging
1g
Price
$300
Updated
2021/12/16
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2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE Chemical Properties,Usage,Production

Synthesis

1194-21-4

1007-99-4

General procedure for the synthesis of 2-amino-4-chloro-5-nitro-6-hydroxypyrimidines from 2-amino-6-chloro-4-hydroxypyrimidines: 2-amino-6-chloropyrimidin-4(3H)-one (10 g, 68.73 mmol) was dissolved in 98% sulfuric acid (46 mL) at 40 °C, keeping stirring. Subsequently, 65% nitric acid (9 g) was slowly added dropwise to the above solution. The reaction mixture was continued to be stirred at room temperature for 1 hour. Upon completion of the reaction, the solution was carefully poured into 100 g of ice to quench the reaction. The precipitate was collected by filtration and the resulting filter cake was dried in a reduced pressure oven to afford 12 g (87% yield) of the target product 2-amino-6-chloro-5-nitropyrimidin-4(3H)-one as a yellow solid. The structure of the product was confirmed by 1H NMR (300 MHz, DMSO-d6): δ 7.13 (1H, s), 8.59 (1H, s), 12.16 (1H, s).

References

[1] Chemistry (Weinheim an der Bergstrasse, Germany), 2002, vol. 8, # 1, p. 293 - 301
[2] Patent: US4939252, 1990, A
[3] Patent: WO2009/139834, 2009, A1. Location in patent: Page/Page column 93-94
[4] Journal of Heterocyclic Chemistry, 1985, vol. 22, # 4, p. 1035 - 1040
[5] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985, p. 1645 - 1660

2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE Suppliers

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View Lastest Price from 2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE manufacturers

Dideu Industries Group Limited
Product
2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE 1007-99-4
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-09
Career Henan Chemical Co
Product
2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE 1007-99-4
Price
US $3.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2020-03-13

1007-99-4, 2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINERelated Search:

2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE NR3 SALT 2-Amino-5-nitropyrimidine 2-Amino-6-chloro-4-pyrimidinol 1-Chloro-2-nitropropane 2-AMINO-6-CHLORO-4-PYRIMIDINOL HYDRATE, 95 2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE

  • ACHNP
  • AKOS 92816
  • 2-AMINO-4-CHLORO-5-NITRO-6-HYDROXYPYRIMIDINE
  • 2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE
  • 2-Amino-6-chloro-5-nitropyrimidin-4(5H)-one
  • 2-amino-6-chloro-5-nitro-1H-pyrimidin-4-one
  • 2-azanyl-6-chloro-5-nitro-1H-pyrimidin-4-one
  • 2-aMino-6-chloro-5-nitro-4-oxo-3,4-dihydro-pyriMidine
  • 2-Amino-6-chloro-5-nitropyrimidin-4-ol
  • 4(1H)-Pyrimidinone,2-amino-6-chloro-5-nitro-
  • 2-Amino-6-chloro-5-nitro-4(3H)-pyrimidone
  • 2-AMINO-4-CHLORO-6-HYDROXY-5-NITROPYRIMIDINE ISO 9001：2015 REACH
  • 2-Amino-6-chloro-5-nitro-4(1H)-pyrimidinone
  • 1007-99-4
  • C4H3ClN4O3