ChemicalBook > CAS DataBase List > 5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL

5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL

Product Name
5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL
CAS No.
17289-30-4
Chemical Name
5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL
Synonyms
4-CHLOROMETHYL-1-METHYL-IMIDAZOLE HCL;4-(CHLOROMETHYL)-1-METHYL-1H-IMIDAZOLE;5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL;4-chloromethyl-1-methyl-imidazole Hydrochloride;5-Chloromethyl-1-methyl-1H-imidazolehydrochloride;4-(ChloroMethyl)-1-Methyl-1H-iMidazole hydrochloride
CBNumber
CB6837224
Molecular Formula
C5H7ClN2
Formula Weight
130.57548
MOL File
17289-30-4.mol
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5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Property

Melting point:
153-154 °C
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC
Product number
C597840
Product name
4-(Chloromethyl)-1-methyl-1H-imidazoleHydrochloride
Packaging
10mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-W007091
Product name
4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
Purity
98.98%
Packaging
100mg
Price
$92
Updated
2021/12/16
ChemScene
Product number
CS-W007091
Product name
4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
Purity
98.98%
Packaging
250mg
Price
$99
Updated
2021/12/16
AK Scientific
Product number
3062CT
Product name
4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
Packaging
100mg
Price
$159
Updated
2021/12/16
ChemScene
Product number
CS-W007091
Product name
4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
Purity
98.98%
Packaging
1g
Price
$278
Updated
2021/12/16
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5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Chemical Properties,Usage,Production

Synthesis

17289-25-7

17289-30-4

At 0 °C, (1-methyl-1H-imidazol-4-yl)methanol (5 g, 44.64 mmol) was dissolved in dichloromethane (10 mL) and thionyl chloride (50 mL) was added slowly and dropwise. The reaction mixture was stirred overnight at room temperature and then refluxed for 3 hours. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure. The residue was treated with diethyl ether and the resulting precipitate was filtered and dried to give 4-(chloromethyl)-1-methyl-1H-imidazole hydrochloride as a brown solid (4 g, 53.80% yield). The product was characterized by 1H NMR (300 MHz, DMSO-d6): δ 9.25 (s, 1H), 7.8 (s, 1H), 4.95 (s, 2H), 3.9 (s, 3H).

References

[1] Patent: WO2004/13134, 2004, A2. Location in patent: Page 26
[2] Patent: WO2004/13135, 2004, A1. Location in patent: Page 47
[3] Patent: WO2004/13138, 2004, A2. Location in patent: Page 23

5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Preparation Products And Raw materials

Raw materials

Preparation Products

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5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Suppliers

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17289-30-4, 5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCLRelated Search:

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  • 4-(CHLOROMETHYL)-1-METHYL-1H-IMIDAZOLE
  • 5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL
  • 5-Chloromethyl-1-methyl-1H-imidazolehydrochloride
  • 4-CHLOROMETHYL-1-METHYL-IMIDAZOLE HCL
  • 4-(ChloroMethyl)-1-Methyl-1H-iMidazole hydrochloride
  • 4-chloromethyl-1-methyl-imidazole Hydrochloride
  • 17289-30-4