5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL
- Product Name
- 5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL
- CAS No.
- 17289-30-4
- Chemical Name
- 5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL
- Synonyms
- 4-CHLOROMETHYL-1-METHYL-IMIDAZOLE HCL;4-(CHLOROMETHYL)-1-METHYL-1H-IMIDAZOLE;5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL;4-chloromethyl-1-methyl-imidazole Hydrochloride;5-Chloromethyl-1-methyl-1H-imidazolehydrochloride;4-(ChloroMethyl)-1-Methyl-1H-iMidazole hydrochloride
- CBNumber
- CB6837224
- Molecular Formula
- C5H7ClN2
- Formula Weight
- 130.57548
- MOL File
- 17289-30-4.mol
5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Property
- Melting point:
- 153-154 °C
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- C597840
- Product name
- 4-(Chloromethyl)-1-methyl-1H-imidazoleHydrochloride
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CS-W007091
- Product name
- 4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
- Purity
- 98.98%
- Packaging
- 100mg
- Price
- $92
- Updated
- 2021/12/16
- Product number
- CS-W007091
- Product name
- 4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
- Purity
- 98.98%
- Packaging
- 250mg
- Price
- $99
- Updated
- 2021/12/16
- Product number
- 3062CT
- Product name
- 4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
- Packaging
- 100mg
- Price
- $159
- Updated
- 2021/12/16
- Product number
- CS-W007091
- Product name
- 4-(Chloromethyl)-1-methyl-1H-imidazolehydrochloride
- Purity
- 98.98%
- Packaging
- 1g
- Price
- $278
- Updated
- 2021/12/16
5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Chemical Properties,Usage,Production
Synthesis
17289-25-7
17289-30-4
At 0 °C, (1-methyl-1H-imidazol-4-yl)methanol (5 g, 44.64 mmol) was dissolved in dichloromethane (10 mL) and thionyl chloride (50 mL) was added slowly and dropwise. The reaction mixture was stirred overnight at room temperature and then refluxed for 3 hours. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure. The residue was treated with diethyl ether and the resulting precipitate was filtered and dried to give 4-(chloromethyl)-1-methyl-1H-imidazole hydrochloride as a brown solid (4 g, 53.80% yield). The product was characterized by 1H NMR (300 MHz, DMSO-d6): δ 9.25 (s, 1H), 7.8 (s, 1H), 4.95 (s, 2H), 3.9 (s, 3H).
References
[1] Patent: WO2004/13134, 2004, A2. Location in patent: Page 26
[2] Patent: WO2004/13135, 2004, A1. Location in patent: Page 47
[3] Patent: WO2004/13138, 2004, A2. Location in patent: Page 23
5-CHLOROMETHYL-1-METHYL-1H-IMIDAZOLE HCL Preparation Products And Raw materials
Raw materials
Preparation Products
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