4-(4-NITRO-BENZOYL)-BENZOIC ACID

Product Name: 4-(4-NITRO-BENZOYL)-BENZOIC ACID
CAS No.: 7377-13-1
Chemical Name: 4-(4-NITRO-BENZOYL)-BENZOIC ACID
Synonyms: 4-(4-Nitrobenzoyl);4-(4-NITRO-BENZOYL)-BENZOIC ACID;Benzoic acid, 4-(4-nitrobenzoyl)-
CBNumber: CB6838342
Molecular Formula: C14H9NO5
Formula Weight: 271.23
MOL File: 7377-13-1.mol

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4-(4-NITRO-BENZOYL)-BENZOIC ACID Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0150334
Product name: 4-(4-NITRO-BENZOYL)-BENZOIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $503.54
Updated: 2021/12/16

AK Scientific

Product number: 9227CB
Product name: 4-(4-Nitrobenzoyl)benzoicacid
Packaging: 10g
Price: $1071
Updated: 2021/12/16

Ambeed

Product number: A278950
Product name: 4-(4-Nitrobenzoyl)benzoicacid
Purity: 96%
Packaging: 250mg
Price: $64
Updated: 2021/12/16

Ambeed

Product number: A278950
Product name: 4-(4-Nitrobenzoyl)benzoicacid
Purity: 96%
Packaging: 1g
Price: $159
Updated: 2021/12/16

Alichem

Product number: 7377131
Product name: 4-(4-Nitrobenzoyl)benzoicacid
Packaging: 1g
Price: $162
Updated: 2021/12/16

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4-(4-NITRO-BENZOYL)-BENZOIC ACID Chemical Properties,Usage,Production

Synthesis

5350-47-0

7377-13-1

General procedure for the synthesis of 4-(4-nitrobenzyl)-benzoic acid from 4-nitrotoluene (CAS: 5350-47-0): Concentrated sulfuric acid (28 mL) was slowly added to a mixture of 4-nitrotoluene (20.00 g, 0.08 mol) and glacial acetic acid (150 mL) under the cooling of an ice bath, and the temperature of the reaction was controlled to be below 5°C. The reaction was carried out in the following manner. Subsequently, chromium oxide (28.00 g, 0.28 mol) was added in small batches at a temperature not exceeding 10 °C. After addition, the reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, ice water (20 mL) was added to the mixture to quench the reaction. The precipitated solid was collected by filtration, washed with water and dried to give 4-(4-nitrobenzyl)-benzoic acid (22.0 g, 85% yield) as a white powder. The melting point of the product was 254-256 °C.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 2, p. 1036 - 1039
[2] Journal of Medicinal Chemistry, 2006, vol. 49, # 2, p. 748 - 759
[3] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 1, p. 380 - 386
[4] Justus Liebigs Annalen der Chemie, 1895, vol. 286, p. 329
[5] Molecular crystals and liquid crystals, 1984, vol. 111, # 3-4, p. 255 - 266

4-(4-NITRO-BENZOYL)-BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(4-NITRO-BENZOYL)-BENZOIC ACID Suppliers

China 25 United Kingdom 1 United States 4 Global 30

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7377-13-1, 4-(4-NITRO-BENZOYL)-BENZOIC ACIDRelated Search:

4-Nitrobenzophenone 4-ETHOXYCARBONYL-4'-NITROBENZOPHENONE 4-BROMOBENZHYDROL NSC62487 4-Acetylbenzoic acid 4-(4-NITRO-BENZOYL)-BENZOIC ACID

4-(4-Nitrobenzoyl)

4-(4-NITRO-BENZOYL)-BENZOIC ACID

Benzoic acid, 4-(4-nitrobenzoyl)-

7377-13-1