4-(4-NITRO-BENZOYL)-BENZOIC ACID
- Product Name
- 4-(4-NITRO-BENZOYL)-BENZOIC ACID
- CAS No.
- 7377-13-1
- Chemical Name
- 4-(4-NITRO-BENZOYL)-BENZOIC ACID
- Synonyms
- 4-(4-Nitrobenzoyl);4-(4-NITRO-BENZOYL)-BENZOIC ACID;Benzoic acid, 4-(4-nitrobenzoyl)-
- CBNumber
- CB6838342
- Molecular Formula
- C14H9NO5
- Formula Weight
- 271.23
- MOL File
- 7377-13-1.mol
4-(4-NITRO-BENZOYL)-BENZOIC ACID Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CHM0150334
- Product name
- 4-(4-NITRO-BENZOYL)-BENZOIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $503.54
- Updated
- 2021/12/16
- Product number
- 9227CB
- Product name
- 4-(4-Nitrobenzoyl)benzoicacid
- Packaging
- 10g
- Price
- $1071
- Updated
- 2021/12/16
- Product number
- 61-10379
- Product name
- 4-(4-Nitrobenzoyl)benzoicacid
- Purity
- 95-98%
- Packaging
- 1g
- Price
- $540
- Updated
- 2021/12/16
- Product number
- CD12037923
- Product name
- 4-(4-Nitrobenzoyl)benzoicacid
- Purity
- 96%
- Packaging
- 10g
- Price
- $713
- Updated
- 2021/12/16
- Product number
- 7377131
- Product name
- 4-(4-Nitrobenzoyl)benzoicacid
- Packaging
- 10g
- Price
- $748.8
- Updated
- 2021/12/16
4-(4-NITRO-BENZOYL)-BENZOIC ACID Chemical Properties,Usage,Production
Synthesis
5350-47-0
7377-13-1
General procedure for the synthesis of 4-(4-nitrobenzyl)-benzoic acid from 4-nitrotoluene (CAS: 5350-47-0): Concentrated sulfuric acid (28 mL) was slowly added to a mixture of 4-nitrotoluene (20.00 g, 0.08 mol) and glacial acetic acid (150 mL) under the cooling of an ice bath, and the temperature of the reaction was controlled to be below 5°C. The reaction was carried out in the following manner. Subsequently, chromium oxide (28.00 g, 0.28 mol) was added in small batches at a temperature not exceeding 10 °C. After addition, the reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, ice water (20 mL) was added to the mixture to quench the reaction. The precipitated solid was collected by filtration, washed with water and dried to give 4-(4-nitrobenzyl)-benzoic acid (22.0 g, 85% yield) as a white powder. The melting point of the product was 254-256 °C.
References
[1] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 2, p. 1036 - 1039
[2] Journal of Medicinal Chemistry, 2006, vol. 49, # 2, p. 748 - 759
[3] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 1, p. 380 - 386
[4] Justus Liebigs Annalen der Chemie, 1895, vol. 286, p. 329
[5] Molecular crystals and liquid crystals, 1984, vol. 111, # 3-4, p. 255 - 266
4-(4-NITRO-BENZOYL)-BENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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