3-(2-BROMO-PHENYL)-PROPAN-1-OL

Product Name: 3-(2-BROMO-PHENYL)-PROPAN-1-OL
CAS No.: 52221-92-8
Chemical Name: 3-(2-BROMO-PHENYL)-PROPAN-1-OL
Synonyms: Benzenepropanol, 2-bromo-;3-(2-BroMophenyl)-1-propanol;3-(2-BROMO-PHENYL)-PROPAN-1-OL;3-(2-Bromophenyl)propan-1-ol,97%;3-(2-Bromophenyl)-1-propanol,98%
CBNumber: CB6839394
Molecular Formula: C9H11BrO
Formula Weight: 215.09
MOL File: 52221-92-8.mol

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3-(2-BROMO-PHENYL)-PROPAN-1-OL Property

Boiling point:: 106-108 °C(Press: 0.5 Torr)
Density: 1.410±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 15.00±0.10(Predicted)
form: Liquid
color: Colorless

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: B698530
Product name: 3-(2-Bromo-phenyl)-propan-1-ol
Packaging: 1g
Price: $75
Updated: 2021/12/16

ChemScene

Product number: CS-W021756
Product name: 3-(2-Bromo-phenyl)-propan-1-ol
Purity: 97.24%
Packaging: 5g
Price: $76
Updated: 2021/12/16

AK Scientific

Product number: J55088
Product name: 3-(2-Bromo-phenyl)-propan-1-ol
Packaging: 5g
Price: $80
Updated: 2021/12/16

AK Scientific

Product number: 7351AB
Product name: 3-(2-Bromo-phenyl)-propan-1-ol
Packaging: 5g
Price: $107
Updated: 2021/12/16

ChemScene

Product number: CS-W021756
Product name: 3-(2-Bromo-phenyl)-propan-1-ol
Purity: 97.24%
Packaging: 10g
Price: $124
Updated: 2021/12/16

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3-(2-BROMO-PHENYL)-PROPAN-1-OL Chemical Properties,Usage,Production

Synthesis

15115-58-9

52221-92-8

General procedure for the synthesis of 2-bromophenylpropanol from 3-(2-bromophenyl)propionic acid: to an anhydrous tetrahydrofuran (5.0 mL) solution of 3-(2-bromophenyl)propionic acid (1.0 g, 4.4 mmol) was slowly added a tetrahydrofuran solution of the borane-tetrahydrofuran complex (1.0 M, 7.0 mL, 7.0 mmol) at 0 °C, and the addition time was controlled at 15 The addition time was controlled to be more than 15 minutes. After addition, the reaction mixture was continued to be stirred at 0 °C for 1 hour. Upon completion of the reaction, the residual borane was quenched by careful addition of water (1 mL) and the solvent was subsequently removed under reduced pressure. The resulting residue was dissolved in ether (20 mL), the organic layer was washed sequentially with water (20 mL) and brine (20 mL), dried over anhydrous sodium sulfate, filtered, and the filtrate was concentrated under reduced pressure to afford 3-(2-bromophenyl)propan-1-ol as a colorless oil (938 mg, quantitative yield). The product did not require further purification and could be used directly in the subsequent reaction.

References

[1] Patent: US2016/95858, 2016, A1. Location in patent: Paragraph 4462; 4463
[2] Journal of Organic Chemistry, 1989, vol. 54, # 23, p. 5574 - 5580
[3] Patent: WO2010/45212, 2010, A2. Location in patent: Page/Page column 222-223
[4] Patent: US2013/184313, 2013, A1. Location in patent: Paragraph 1274; 1275
[5] Angewandte Chemie - International Edition, 2018, vol. 57, # 18, p. 5124 - 5128

3-(2-BROMO-PHENYL)-PROPAN-1-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(2-BROMO-PHENYL)-PROPAN-1-OL Suppliers

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View Lastest Price from 3-(2-BROMO-PHENYL)-PROPAN-1-OL manufacturers

Career Henan Chemical Co

Product: 3-(2-BROMO-PHENYL)-PROPAN-1-OL 52221-92-8
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

52221-92-8, 3-(2-BROMO-PHENYL)-PROPAN-1-OLRelated Search:

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3-(2-BROMO-PHENYL)-PROPAN-1-OL

3-(2-BroMophenyl)-1-propanol

Benzenepropanol, 2-bromo-

3-(2-Bromophenyl)-1-propanol,98%

3-(2-Bromophenyl)propan-1-ol,97%

52221-92-8