5-CHLORO-3-IODO-2-METHYLANILINE

Product Name: 5-CHLORO-3-IODO-2-METHYLANILINE
CAS No.: 870606-29-4
Chemical Name: 5-CHLORO-3-IODO-2-METHYLANILINE
Synonyms: 5-CHLORO-3-IODO-2-METHYLANILINE;5-Chloro-3-iodo-2-methylbenzenamine;Benzenamine, 5-chloro-3-iodo-2-methyl-
CBNumber: CB6846336
Molecular Formula: C7H7ClIN
Formula Weight: 267.49
MOL File: 870606-29-4.mol

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5-CHLORO-3-IODO-2-METHYLANILINE Property

Boiling point:: 327.8±42.0 °C(Predicted)
Density: 1.883±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.43±0.10(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 3727AC
Product name: 5-Chloro-3-iodo-2-methylaniline
Packaging: 100mg
Price: $142
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0105199
Product name: 5-CHLORO-3-IODO-2-METHYLANILINE
Purity: 95.00%
Packaging: 250MG
Price: $362.25
Updated: 2021/12/16

Chemenu

Product number: CM128940
Product name: 5-chloro-3-iodo-2-methylaniline
Purity: 95+%
Packaging: 5g
Price: $608
Updated: 2021/12/16

Crysdot

Product number: CD12021823
Product name: 5-Chloro-3-iodo-2-methylaniline
Purity: 98%
Packaging: 5g
Price: $644
Updated: 2021/12/16

Alichem

Product number: 870606294
Product name: 5-Chloro-3-iodo-2-methylaniline
Packaging: 5g
Price: $907.99
Updated: 2021/12/16

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5-CHLORO-3-IODO-2-METHYLANILINE Chemical Properties,Usage,Production

Synthesis

294190-16-2

870606-29-4

The general procedure for the synthesis of 5-chloro-3-iodo-2-methyl-3-nitrobenzene from 5-chloro-1-iodo-2-methyl-3-nitrobenzene was as follows: 5-chloro-1-iodo-2-methyl-3-nitrobenzene (3.0 g, 10.1 mmol) was mixed with tin(II) chloride dihydrate (9.1 g, 40.4 mmol) in acetic acid (10 mL) and stirred for 1 hour at room temperature. After the reaction was completed, the reaction mixture was diluted with ether. The mixture was cooled to 0°C and 50% aqueous sodium hydroxide solution was added slowly. The lumpy white solid generated in the reaction was removed by filtration. The filtrate was concentrated and the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate, 4:1, v/v) to afford 5-chloro-3-iodo-2-methylaniline (1.81 g, 67% yield) as a light yellow solid.1H NMR (400 MHz, CDCl3) δ 7.25 (d, 1H), 6.64 (d, 1H), 3.78 (br s 2H), 2.28 (s, 3H).

References

[1] Patent: WO2005/117909, 2005, A2. Location in patent: Page/Page column 113

5-CHLORO-3-IODO-2-METHYLANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-CHLORO-3-IODO-2-METHYLANILINE Suppliers

China 25 India 2 United States 5 Global 32

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View Lastest Price from 5-CHLORO-3-IODO-2-METHYLANILINE manufacturers

Career Henan Chemica Co

Product: 5-CHLORO-3-IODO-2-METHYLANILINE 870606-29-4
Price: US $1.00/g
Min. Order: 1g
Purity: Min98% HPLC/GC
Supply Ability: g/kg/ton Coreychem-Nicole
Release date: 2020-11-06

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-CHLORO-3-IODO-2-METHYLANILINE 870606-29-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-CHLORO-3-IODO-2-METHYLANILINE 870606-29-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

870606-29-4, 5-CHLORO-3-IODO-2-METHYLANILINERelated Search:

2-AMINO-6-IODOTOLUENE 4-CHLORO-2-IODO-6-NITROTOLUENE 5-CHLORO-3-IODO-2-METHYLANILINE 4-CHLORO-2-IODOTOLUENE

5-CHLORO-3-IODO-2-METHYLANILINE

5-Chloro-3-iodo-2-methylbenzenamine

Benzenamine, 5-chloro-3-iodo-2-methyl-

870606-29-4