5-CHLORO-3-IODO-2-METHYLANILINE
- Product Name
- 5-CHLORO-3-IODO-2-METHYLANILINE
- CAS No.
- 870606-29-4
- Chemical Name
- 5-CHLORO-3-IODO-2-METHYLANILINE
- Synonyms
- 5-CHLORO-3-IODO-2-METHYLANILINE;5-Chloro-3-iodo-2-methylbenzenamine;Benzenamine, 5-chloro-3-iodo-2-methyl-
- CBNumber
- CB6846336
- Molecular Formula
- C7H7ClIN
- Formula Weight
- 267.49
- MOL File
- 870606-29-4.mol
5-CHLORO-3-IODO-2-METHYLANILINE Property
- Boiling point:
- 327.8±42.0 °C(Predicted)
- Density
- 1.883±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 2.43±0.10(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 3727AC
- Product name
- 5-Chloro-3-iodo-2-methylaniline
- Packaging
- 100mg
- Price
- $142
- Updated
- 2021/12/16
- Product number
- HCH0105199
- Product name
- 5-CHLORO-3-IODO-2-METHYLANILINE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $362.25
- Updated
- 2021/12/16
- Product number
- CM128940
- Product name
- 5-chloro-3-iodo-2-methylaniline
- Purity
- 95+%
- Packaging
- 5g
- Price
- $608
- Updated
- 2021/12/16
- Product number
- CD12021823
- Product name
- 5-Chloro-3-iodo-2-methylaniline
- Purity
- 98%
- Packaging
- 5g
- Price
- $644
- Updated
- 2021/12/16
- Product number
- 870606294
- Product name
- 5-Chloro-3-iodo-2-methylaniline
- Packaging
- 5g
- Price
- $907.99
- Updated
- 2021/12/16
5-CHLORO-3-IODO-2-METHYLANILINE Chemical Properties,Usage,Production
Synthesis
294190-16-2
870606-29-4
The general procedure for the synthesis of 5-chloro-3-iodo-2-methyl-3-nitrobenzene from 5-chloro-1-iodo-2-methyl-3-nitrobenzene was as follows: 5-chloro-1-iodo-2-methyl-3-nitrobenzene (3.0 g, 10.1 mmol) was mixed with tin(II) chloride dihydrate (9.1 g, 40.4 mmol) in acetic acid (10 mL) and stirred for 1 hour at room temperature. After the reaction was completed, the reaction mixture was diluted with ether. The mixture was cooled to 0°C and 50% aqueous sodium hydroxide solution was added slowly. The lumpy white solid generated in the reaction was removed by filtration. The filtrate was concentrated and the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate, 4:1, v/v) to afford 5-chloro-3-iodo-2-methylaniline (1.81 g, 67% yield) as a light yellow solid.1H NMR (400 MHz, CDCl3) δ 7.25 (d, 1H), 6.64 (d, 1H), 3.78 (br s 2H), 2.28 (s, 3H).
References
[1] Patent: WO2005/117909, 2005, A2. Location in patent: Page/Page column 113
5-CHLORO-3-IODO-2-METHYLANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
5-CHLORO-3-IODO-2-METHYLANILINE Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 5-CHLORO-3-IODO-2-METHYLANILINE manufacturers
- Product
- 5-CHLORO-3-IODO-2-METHYLANILINE 870606-29-4
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- Min98% HPLC/GC
- Supply Ability
- g/kg/ton Coreychem-Nicole
- Release date
- 2020-11-06
- Product
- 5-CHLORO-3-IODO-2-METHYLANILINE 870606-29-4
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
- Product
- 5-CHLORO-3-IODO-2-METHYLANILINE 870606-29-4
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09