3-bromo-5-methylaniline

Product Name: 3-bromo-5-methylaniline
CAS No.: 74586-53-1
Chemical Name: 3-bromo-5-methylaniline
Synonyms: 3-AMino-5-broMotoluene;3-bromo-5-methylaniline;3-Bromo-5-methylbenzenamine;3-Bromo-5-methylaniline,98%;BenzenaMine,3-broMo-5-Methyl-;3-Amino-5-bromotoluene, 5-Bromo-m-toluidine
CBNumber: CB6908751
Molecular Formula: C7H8BrN
Formula Weight: 186.05
MOL File: 74586-53-1.mol

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3-bromo-5-methylaniline Property

Melting point:: 37 °C
Boiling point:: 150-151 °C(Press: 15 Torr)
Density: 1.498±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: Powder
pka: 3.65±0.10(Predicted)
color: Brown
Water Solubility: Slightly soluble in water.

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Safety

HazardClass: 6.1
HS Code: 2921430090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B6015
Product name: 3-Bromo-5-methylaniline
Packaging: 5G
Price: $157
Updated: 2025/07/31

TCI Chemical

Product number: B6015
Product name: 3-Bromo-5-methylaniline
Packaging: 25G
Price: $626
Updated: 2025/07/31

TRC

Product number: B814220
Product name: 3-Bromo-5-methylaniline
Packaging: 10g
Price: $200
Updated: 2021/12/16

Matrix Scientific

Product number: 074390
Product name: 3-Bromo-5-methylaniline
Purity: 95+%
Packaging: 25g
Price: $218
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140428
Product name: 3-Bromo-5-methylaniline
Packaging: 25g
Price: $224
Updated: 2021/12/16

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3-bromo-5-methylaniline Chemical Properties,Usage,Production

Uses

3-Bromo-5-methylaniline is used as pharmaceutical intermediates and chemical intermediate.

Synthesis

52488-28-5

74586-53-1

General procedure for the synthesis of 3-bromo-5-methylaniline from 3-bromo-5-nitrotoluene: 1-bromo-3-methyl-5-nitrobenzene (5 g, 23.1 mmol) was dissolved in a mixed solvent of dioxane/water (3:1, 40 mL), and zinc powder (15 g, 231 mmol) and ammonium chloride (12.3 g, 231 mmol) were added sequentially. The reaction mixture was stirred at room temperature for 4 hours. After completion of the reaction, the reaction mixture was diluted with water and extracted with ethyl acetate. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 3-bromo-5-methylaniline (4.0 g, 93% yield) as a brown solid. Mass spectrometry analysis showed m/z (M+H) of 186.2.

References

[1] Patent: WO2014/149164, 2014, A1. Location in patent: Paragraph 001105
[2] Chemische Berichte, 1880, vol. 13, p. 963
[3] Chemische Berichte, 1881, vol. 14, p. 417
[4] Justus Liebigs Annalen der Chemie, 1878, vol. 192, p. 203
[5] Journal of the Chemical Society, 1929, p. 1255

3-bromo-5-methylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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3-bromo-5-methylaniline Suppliers

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View Lastest Price from 3-bromo-5-methylaniline manufacturers

Career Henan Chemical Co

Product: 3-bromo-5-methylaniline 74586-53-1
Price: US $7.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: JD724
Release date: 2019-09-02

74586-53-1, 3-bromo-5-methylanilineRelated Search:

3-bromo-5-methylaniline

3-Bromo-5-methylbenzenamine

3-Amino-5-bromotoluene, 5-Bromo-m-toluidine

3-AMino-5-broMotoluene

BenzenaMine,3-broMo-5-Methyl-

3-Bromo-5-methylaniline,98%

74586-53-1

277-932-1