2-isopropoxyaniline
- Product Name
- 2-isopropoxyaniline
- CAS No.
- 29026-74-2
- Chemical Name
- 2-isopropoxyaniline
- Synonyms
- o-Ipa;o-Isopropoxyaniline;ANILINE, o-ISOPROPOXY-;2-(1-Methylethoxy)aniline;2-(propan-2-yloxy)aniline;2-(1-Methylethoxy)benzenamine;o-Izopropoksyanilina [Polish];Benzenamine, 2-(1-methylethoxy)-;(2-isopropoxyphenyl)amine sulfate;(2-isopropoxyphenyl)amine(SALTDATA: HCl)
- CBNumber
- CB6915021
- Molecular Formula
- C9H13NO
- Formula Weight
- 151.21
- MOL File
- 29026-74-2.mol
2-isopropoxyaniline Property
- Melting point:
- 139-141℃
- Boiling point:
- 273.23°C (rough estimate)
- Density
- 1.0406 (rough estimate)
- refractive index
- 1.5380 (estimate)
- storage temp.
- 2-8°C(protect from light)
- form
- solid
- pka
- 5.17±0.10(Predicted)
- Appearance
- Brown to black Liquid
Safety
- HazardClass
- IRRITANT
- HS Code
- 2922290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 033964
- Product name
- 2-Isopropoxy-phenylamine
- Packaging
- 1g
- Price
- $73
- Updated
- 2021/12/16
- Product number
- W5162
- Product name
- 2-Isopropoxyaniline
- Packaging
- 5g
- Price
- $169
- Updated
- 2021/12/16
- Product number
- 033964
- Product name
- 2-Isopropoxy-phenylamine
- Packaging
- 5g
- Price
- $235
- Updated
- 2021/12/16
- Product number
- W5162
- Product name
- 2-Isopropoxyaniline
- Packaging
- 25g
- Price
- $454
- Updated
- 2021/12/16
- Product number
- CHM0032774
- Product name
- (2-ISOPROPOXY PHENYL)AMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $765.23
- Updated
- 2021/12/16
2-isopropoxyaniline Chemical Properties,Usage,Production
Synthesis
38753-50-3
29026-74-2
General procedure for the synthesis of 2-(1-methylethoxy)aniline from 1-isopropoxy-2-nitrobenzene: The product of Example 242A (5.00 g, 27.5 mmol) was dissolved in methanol, 10% Pd/C catalyst was added, and the catalytic hydrogenation reaction was carried out under hydrogen pressure (60 psi). Upon completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to afford 3.75 g (90% yield) of the target product 2-(1-methylethoxy)aniline in the form of a brown oil. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 1.35 (d, 6H, J = 6.1 Hz), 3.77 (br s, 2H), 4.52 (m, 1H), 6.75 (m, 4H); the mass spectrum (DCI/NH3) showed m/e 152 (M + H)+.
References
[1] Organic Letters, 2011, vol. 13, # 16, p. 4320 - 4323
[2] Patent: US2003/229094, 2003, A1. Location in patent: Page 107
[3] Patent: WO2005/113498, 2005, A1. Location in patent: Page/Page column 16
[4] Patent: WO2014/11973, 2014, A2. Location in patent: Paragraph 0157; 0161
[5] Bioorganic and medicinal chemistry, 2004, vol. 12, # 16, p. 4511 - 4532
2-isopropoxyaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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