2-Bromo-6-nitrobenzaldehyde
- Product Name
- 2-Bromo-6-nitrobenzaldehyde
- CAS No.
- 20357-21-5
- Chemical Name
- 2-Bromo-6-nitrobenzaldehyde
- Synonyms
- 100117;2-Bromo-6-nitrobenzaldehyde;3-Amino-5-chloroacetophenone;Benzaldehyde, 2-broMo-6-nitro-;2-Bromo-6-nitrobenzaldehyde 98%;2-Bromo-6-Nitrobenzaldehyde,>98%
- CBNumber
- CB6947004
- Molecular Formula
- C7H4BrNO3
- Formula Weight
- 230.02
- MOL File
- 20357-21-5.mol
2-Bromo-6-nitrobenzaldehyde Property
- Melting point:
- 86-87°C
- Boiling point:
- 320.8±27.0 °C(Predicted)
- Density
- 1.781
- refractive index
- 1.653
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- color
- Yellow
- InChI
- InChI=1S/C7H4BrNO3/c8-6-2-1-3-7(9(11)12)5(6)4-10/h1-4H
- InChIKey
- WRIAMYXQKSDDRP-UHFFFAOYSA-N
- SMILES
- C(=O)C1=C([N+]([O-])=O)C=CC=C1Br
Safety
- HS Code
- 2913000090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B694745
- Product name
- 2-Bromo-6-nitrobenzaldehyde
- Packaging
- 1g
- Price
- $145
- Updated
- 2021/12/16
- Product number
- FB05063
- Product name
- 2-Bromo-6-nitrobenzaldehyde
- Packaging
- 2g
- Price
- $320
- Updated
- 2021/12/16
- Product number
- FB05063
- Product name
- 2-Bromo-6-nitrobenzaldehyde
- Packaging
- 1g
- Price
- $220
- Updated
- 2021/12/16
- Product number
- HCH0036769
- Product name
- 2-BROMO-6-NITROBENZALDEHYDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $240.45
- Updated
- 2021/12/16
- Product number
- 071169
- Product name
- 2-Bromo-6-nitrobenzaldehyde
- Purity
- 97%
- Packaging
- 5g
- Price
- $272
- Updated
- 2021/12/16
2-Bromo-6-nitrobenzaldehyde Chemical Properties,Usage,Production
Uses
2-Bromo-6-nitrobenzaldehyde is mainly used as an intermediate in organic synthesis, especially in the production of drugs and dyes.
Synthesis
N-Bromosuccinimide (NBS) (1.48 g, 8.32 mmol) was added to a solution of 2-Nitrobenzaldehyde (1.01 g, 6.71 mmol) in H2SO4 (concentrated 5.0 mL). The resulting mixture was stirred at ambient temperature (3 h). The reaction was quenched with ice and extracted with ethyl acetate (320mL). The combined organic phases were washed with saturated NaCl (aqueous, 30 mL), dried (MgSO4), and filtered through a silica gel plug, and the solvents were evaporated under reduced pressure. The resulting brown oil was purified by column chromatography (hexanes=EtOAc, 8:2) to afford 2-Bromo-6-nitrobenzaldehyde.
References
[1] Patent: WO2008/156656, 2008, A2. Location in patent: Page/Page column 58; 66; 120
2-Bromo-6-nitrobenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Bromo-6-nitrobenzaldehyde manufacturers
- Product
- 2-Bromo-6-nitrobenzaldehyde 20357-21-5
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99.99%
- Supply Ability
- 50000tons
- Release date
- 2023-08-15
- Product
- 2-Bromo-6-nitrobenzaldehyde 20357-21-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-12