4-IODO-2-METHOXYPYRIDINE
- Product Name
- 4-IODO-2-METHOXYPYRIDINE
- CAS No.
- 98197-72-9
- Chemical Name
- 4-IODO-2-METHOXYPYRIDINE
- Synonyms
- 4-Iodo-2-methoxypyridine;4-Iodo-2-methoxypyridinev;Pyridine,4-iodo-2-Methoxy-;4-Iodo-2-methoxypyridine 98%;(2-iodo-pyridin-4-yl)-dimethyl-amine
- CBNumber
- CB71010663
- Molecular Formula
- C6H6INO
- Formula Weight
- 235.02
- MOL File
- 98197-72-9.mol
4-IODO-2-METHOXYPYRIDINE Property
- Boiling point:
- 106 °C(Press: 15 Torr)
- Density
- 1.825±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 2.02±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I708650
- Product name
- 4-Iodo-2-methoxypyridine
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- J51597
- Product name
- 4-Iodo-2-methoxypyridine
- Packaging
- 1g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- V1745
- Product name
- 4-Iodo-2-methoxypyridine
- Packaging
- 1g
- Price
- $95
- Updated
- 2021/12/16
- Product number
- 4H56-H-31
- Product name
- 4-Iodo-2-methoxypyridine
- Packaging
- 1g
- Price
- $108
- Updated
- 2021/12/16
- Product number
- 074489
- Product name
- 4-Iodo-2-methoxypyridine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $416
- Updated
- 2021/12/16
4-IODO-2-METHOXYPYRIDINE Chemical Properties,Usage,Production
Synthesis
67-56-1
124-41-4
22282-70-8
98197-72-9
(C) 500 mL of methanol was added to 59.4 g (253 mmol) of crude 2-fluoro-4-iodopyridine obtained from step (B) and stirred until completely dissolved. Subsequently 21.5 g (398 mmol) of sodium methanol was added and the reaction was heated to reflux for 3 hours. Upon completion of the reaction, 300 mL of water was added to quench the reaction, followed by removal of methanol by distillation under reduced pressure. The reaction mixture was extracted with ether and the organic layers were combined and dried over anhydrous sodium sulfate. After filtration, the solvent was removed by reduced pressure distillation to afford the crude product 4-iodo-2-methoxypyridine 56.7 g (crude yield: 91%). The structure of the product was confirmed by 1H-NMR (CDCl3, 400 MHz): δ (ppm) = 3.86 (s, 3H), 7.12-7.16 (m, 2H), 7.79 (d, 1H, J = 5.6 Hz).
References
[1] Patent: EP1679003, 2006, A1. Location in patent: Page/Page column 13
4-IODO-2-METHOXYPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
4-IODO-2-METHOXYPYRIDINE Suppliers
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View Lastest Price from 4-IODO-2-METHOXYPYRIDINE manufacturers
- Product
- 4-IODO-2-METHOXYPYRIDINE 98197-72-9
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-14
- Product
- 4-IODO-2-METHOXYPYRIDINE 98197-72-9
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-09-02
- Product
- 4-Iodo-2-methoxypyridine 98197-72-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10