Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)

Product Name: Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
CAS No.: 30152-05-7
Chemical Name: Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
Synonyms: 1-(3-Hydroxypyridin-4-yl);4-ACETYL-3-HYDROXYPYRIDINE;1-(3-hydroxy-4-pyridyl)ethanone;3-hydroxy-4-pyridylmethyl ketone;1-(3-Hydroxypyridin-4-yl)ethanone;1-(3-Hydroxy-4-pyridinyl)ethanone;1-(3-hydroxypyridin-4-yl)ethan-1-one;Ethanone, 1-(3-hydroxy-4-pyridinyl)-;Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
CBNumber: CB71066064
Molecular Formula: C7H7NO2
Formula Weight: 137.14
MOL File: 30152-05-7.mol

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Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Property

Melting point:: 52-54℃
Boiling point:: 336.5±22.0 °C(Predicted)
Density: 1.217±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 6.90±0.10(Predicted)
Appearance: Yellow to brown Solid
InChI: InChI=1S/C7H7NO2/c1-5(9)6-2-3-8-4-7(6)10/h2-4,10H,1H3
InChIKey: REYSBWKWFPSDDR-UHFFFAOYSA-N
SMILES: C(=O)(C1C=CN=CC=1O)C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: A416805
Product name: 1-(3-Hydroxypyridin-4-yl)ethanone
Packaging: 50mg
Price: $90
Updated: 2021/12/16

TRC

Product number: A416805
Product name: 1-(3-Hydroxypyridin-4-yl)ethanone
Packaging: 100mg
Price: $130
Updated: 2021/12/16

ChemScene

Product number: CS-B0938
Product name: Ethanone,1-(3-hydroxy-4-pyridinyl)-
Purity: 99.96%
Packaging: 100mg
Price: $84
Updated: 2021/12/16

ChemScene

Product number: CS-B0938
Product name: Ethanone,1-(3-hydroxy-4-pyridinyl)-
Purity: 99.96%
Packaging: 250mg
Price: $136
Updated: 2021/12/16

AK Scientific

Product number: Z4577
Product name: 1-(3-Hydroxypyridin-4-yl)ethanone
Packaging: 100mg
Price: $171
Updated: 2021/12/16

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Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

1089689-12-2

30152-05-7

Synthesis of Intermediate IV: Intermediate III (6 g, 33.114 mmol, 1 eq.) was dissolved in EtOH (96 mL), followed by addition of 5 M hydrochloric acid (53 mL). The reaction mixture was stirred at room temperature for 16 hours. Upon completion of the reaction, the solvent was removed by evaporation and the residue was dissolved in MeOH, added to silica gel and evaporated again. Purification by fast chromatography (Biotage, eluent 0% to 20% MeOH in DCM solution) gave Intermediate IV (4.5 g, 99% yield) in orange solid form. The product was analyzed by HPLC-MS (Method 4): retention time Rt = 0.7, [M + H]+ 138.1.1. 1H NMR (300 MHz, DMSO) δ 8.58 (s, 1H), 8.33 (d, J = 4.9 Hz, 1H), 7.80 (d, J = 5.3 Hz, 1H), 2.64 (s, 3H).

References

[1] Patent: WO2017/33019, 2017, A1. Location in patent: Page/Page column 69; 70
[2] Patent: WO2014/141110, 2014, A2. Location in patent: Page/Page column 97

Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Suppliers

China 63 Europe 1 India 2 Switzerland 1 United Kingdom 1 United States 6 Global 74

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View Lastest Price from Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) 30152-05-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-07-18

Career Henan Chemical Co

Product: Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) 30152-05-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-02

30152-05-7, Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)Related Search:

Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)

4-ACETYL-3-HYDROXYPYRIDINE

1-(3-Hydroxypyridin-4-yl)ethanone

Ethanone, 1-(3-hydroxy-4-pyridinyl)-

1-(3-Hydroxy-4-pyridinyl)ethanone

3-hydroxy-4-pyridylmethyl ketone

1-(3-Hydroxypyridin-4-yl)

1-(3-hydroxy-4-pyridyl)ethanone

1-(3-hydroxypyridin-4-yl)ethan-1-one

30152-05-7

ACETYLGROUP