2-BROMO-3-CHLOROANILINE
- Product Name
- 2-BROMO-3-CHLOROANILINE
- CAS No.
- 96558-73-5
- Chemical Name
- 2-BROMO-3-CHLOROANILINE
- Synonyms
- 2-BROMO-3-CHLOROANILINE;2-broMo-3-chlorobenzenaMine;Benzenamine, 2-bromo-3-chloro;(2-Bromo-3-chlorophenyl)amine;BENZENAMINE,2-BROMO-3-CHLORO,2-Bromo-3-chloro-phenylamine,2-BROMO-3-CHLOROBENZENAMINE
- CBNumber
- CB71092742
- Molecular Formula
- C6H5BrClN
- Formula Weight
- 206.47
- MOL File
- 96558-73-5.mol
2-BROMO-3-CHLOROANILINE Property
- Melting point:
- 41-43℃
- Boiling point:
- 277℃
- Density
- 1.722
- Flash point:
- 122℃
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- crystalline solid
- pka
- 1.48±0.10(Predicted)
- color
- Light to dark brown
- InChI
- InChI=1S/C6H5BrClN/c7-6-4(8)2-1-3-5(6)9/h1-3H,9H2
- InChIKey
- JHHMLFBYFNAPDZ-UHFFFAOYSA-N
- SMILES
- C1(N)=CC=CC(Cl)=C1Br
Safety
- RIDADR
- 2811
- HazardClass
- 6.1
- PackingGroup
- Ⅲ
- HS Code
- 2921420090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B415965
- Product name
- 2-Bromo-3-chloroaniline
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- B415965
- Product name
- 2-Bromo-3-chloroaniline
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 075474
- Product name
- 2-Bromo-3-chloroaniline
- Purity
- 95+%
- Packaging
- 1g
- Price
- $20
- Updated
- 2021/12/16
- Product number
- 078926
- Product name
- 2-Bromo-3-chloroaniline
- Purity
- 98%
- Packaging
- 1g
- Price
- $20
- Updated
- 2021/12/16
- Product number
- J91343
- Product name
- 2-Bromo-3-chloroaniline
- Packaging
- 1g
- Price
- $20
- Updated
- 2021/12/16
2-BROMO-3-CHLOROANILINE Chemical Properties,Usage,Production
Chemical Properties
2-Bromo-3-chloroaniline exhibits nonpolar properties, which allows it to bind to the stationary phase of the column and act as an electron scavenger. It reacts with the electrons released by the sample components, resulting in a measurable current.
Uses
2-Bromo-3-chloroaniline is a bromoderivative that is used as an electron detector in gas chromatography. It can also be used as an indicator for bromination reactions.
Synthesis
1463053-89-5
96558-73-5
Step B: Synthesis of 2-bromo-3-chloroaniline To a solution of tert-butyl (2-bromo-3-chlorophenyl)carbamate (0.4 g) in dichloromethane (DCM, 20 mL) was added trifluoroacetic acid (TFA, 10 mL). The reaction mixture was stirred at room temperature for 3 h. The reaction solution was subsequently concentrated by rotary evaporator. Water (10 mL) was added to the concentrated residue and the mixture was extracted with dichloromethane (2 x 20 mL). The organic phase was separated and washed sequentially with saturated aqueous sodium bicarbonate (NaHCO3) and saturated aqueous sodium chloride (NaCl), dried over anhydrous sodium sulfate (Na2SO4), and then the organic phase was concentrated to give the title compound 2-bromo-3-chloroaniline as a solid (0.2 g, 77% yield). 1H NMR (400 MHz, CDCl3) δ 7.03-6.99 (1H, m), 6.85-6.83 (1H, d, J = 8.0 Hz), 6.65-6.63 (1H, d, J = 8.0 Hz), 4.25 (2H, s).
References
[1] Patent: WO2013/148603, 2013, A1. Location in patent: Paragraph 0185-0186
2-BROMO-3-CHLOROANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-BROMO-3-CHLOROANILINE manufacturers
- Product
- 2-BROMO-3-CHLOROANILINE 96558-73-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-11