Methyl quinoline-5-carboxylate

Product Name: Methyl quinoline-5-carboxylate
CAS No.: 16675-62-0
Chemical Name: Methyl quinoline-5-carboxylate
Synonyms: Methyl 5-quinolinecarboxylate;Methyl quinoline-5-carboxylate;Quinoline-5-carboxylic acid Methyl ester;5-Quinoline-carboxylic acid methyl ester;Methyl quinoline-5-carboxylate ISO 9001：2015 REACH
CBNumber: CB71118330
Molecular Formula: C11H9NO2
Formula Weight: 187.19
MOL File: 16675-62-0.mol

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Methyl quinoline-5-carboxylate Property

Melting point:: 51-52 °C(Solv: hexane (110-54-3))
Boiling point:: 315.1±15.0 °C(Predicted)
Density: 1.210±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 3.84±0.12(Predicted)

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M356960
Product name: methylquinoline-5-carboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR940019
Product name: Methylquinoline-5-carboxylate
Purity: 98%
Packaging: 250mg
Price: $80
Updated: 2021/12/16

Matrix Scientific

Product number: 083544
Product name: Methyl quinoline-5-carboxylate
Purity: 97%
Packaging: 1g
Price: $341
Updated: 2021/12/16

Apolloscientific

Product number: OR940019
Product name: Methylquinoline-5-carboxylate
Purity: 98%
Packaging: 1g
Price: $180
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0118908
Product name: METHYL QUINOLINE-5-CARBOXYLATE
Purity: 95.00%
Packaging: 1G
Price: $721.57
Updated: 2021/12/16

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Methyl quinoline-5-carboxylate Chemical Properties,Usage,Production

Synthesis

67-56-1

99-05-8

56-81-5

16675-62-0

Synthesis of methyl quinoline-5-carboxylate (Intermediate-97): To a 500 mL round-bottom flask equipped with a magnetic stirrer was added 90 mL of concentrated sulfuric acid solution of m-aminobenzoic acid (60 g, 435 mmol), glycerol (168 g, 1824 mmol) and 3-nitrobenzoic acid (30 g, 179 mmol). The reaction mixture was heated and stirred at 150°C for 7 hours. Upon completion of the reaction, the mixture was cooled to room temperature, methanol (600 mL) was added and refluxed for 12 hours. Subsequently, the mixture was cooled to 0°C, the reaction was quenched with ice water and concentrated under reduced pressure. The crude product was alkalized with aqueous sodium bicarbonate, extracted with dichloromethane and concentrated by combining the organic phases. The crude product was purified by silica gel column chromatography with the eluent being a solvent mixture of petroleum ether (60-80°C fraction), ethyl acetate and 0.5% triethylamine. Methyl quinoline-5-carboxylate (Intermediate-97) was finally obtained as a brown liquid (21 g).

References

[1] Patent: WO2013/128465, 2013, A1. Location in patent: Page/Page column 203
[2] Patent: US2015/158860, 2015, A1. Location in patent: Paragraph 0750; 0751

Methyl quinoline-5-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl quinoline-5-carboxylate Suppliers

China 61 Germany 1 India 1 Ukraine 2 United Kingdom 1 United States 9 Global 75

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View Lastest Price from Methyl quinoline-5-carboxylate manufacturers

Career Henan Chemical Co

Product: Methyl quinoline-5-carboxylate 16675-62-0
Price: US $1.00/KG
Min. Order: 1g
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-09

16675-62-0, Methyl quinoline-5-carboxylateRelated Search:

Quinoline-5-carboxaldehyde Methyl quinoline-5-carboxylate ETHYL QUINOLINE-5-CARBOXYLATE ISOQUINOLINE-5-CARBOXYLIC ACID 5-HYDROXYMETHYLQUINOLINE

Methyl quinoline-5-carboxylate

5-Quinoline-carboxylic acid methyl ester

Methyl 5-quinolinecarboxylate

Quinoline-5-carboxylic acid Methyl ester

Methyl quinoline-5-carboxylate ISO 9001：2015 REACH

16675-62-0

Esters

Quinolines, Isoquinolines & Quinoxalines