Methyl p-nitrophenylacetate

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Methyl p-nitrophenylacetate

Appearance

Product Name: Methyl p-nitrophenylacetate
CAS No.: 2945-08-6
Chemical Name: Methyl p-nitrophenylacetate
Synonyms: Methyl 2-(4-nitrophenyl);Methyl p-nitrophenylacetate;Methyl 2-(4-nitrophenyl)acetate;4-Nitrophenylacetic acid methyl ester;4-Nitrobenzeneacetic acid methyl ester;(4-Nitrophenyl)acetic acid methyl ester;2-(p-Nitrophenyl)acetic acid methyl ester;Benzeneacetic acid, 4-nitro-, methyl ester
CBNumber: CB71180214
Molecular Formula: C9H9NO4
Formula Weight: 195.17
MOL File: 2945-08-6.mol

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Methyl p-nitrophenylacetate Property

Melting point:: 52.4-53.3 °C
Boiling point:: 308.6±17.0 °C(Predicted)
Density: 1.266±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: solid
color: Off-white

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Safety

HS Code: 2915390090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 2998AB
Product name: Methyl2-(4-nitrophenyl)acetate
Packaging: 5g
Price: $171
Updated: 2021/12/16

Matrix Scientific

Product number: 113919
Product name: Methyl (4-nitrophenyl)acetate
Purity: 97%
Packaging: 1g
Price: $354
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0392884
Product name: METHYL-2-(4-NITROPHENYL)ACETATE
Purity: 95.00%
Packaging: 5MG
Price: $504.09
Updated: 2021/12/16

AK Scientific

Product number: 4995AQ
Product name: methyl2-(4-nitrophenyl)acetate
Packaging: 25g
Price: $590
Updated: 2021/12/16

Alichem

Product number: 2945086
Product name: Methyl2-(4-nitrophenyl)acetate
Packaging: 25g
Price: $366.12
Updated: 2021/12/16

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Methyl p-nitrophenylacetate Chemical Properties,Usage,Production

Appearance

a pale orange oil

Synthesis

4-nitrophenylacetic acid(2.00 g, 11 mmol) was added to a clean carousel tube. Dimethyl carbonate (3 mL, 3.21 g, 35.6 mmol) was added, and the reaction was heated at reflux overnight. The brown solution was allowed to cool, and poured in to aqueous sodium bicarbonate (10%, 10 mL) while stirring. The resulting mixture was extracted with ethyl acetate (3 x 10 mL). The combined organic layers were washed with water and brine (10 mL each), and dried over anhydrous magnesium sulphate. After filtration and evaporation of the solvents, proton NMR analysis showed the product had formed, and none of the precursor acid remained. No further purification was performed. This gave methyl p-nitrophenylacetate as a pale orange oil (1.929 g, 9.89 mmol, 90%)): 1H NMR (400 MHz, CDCl 3 ) |? 8.20 (d, J = 8.6 Hz, 2H), 7.46 (d, J = 8.6 Hz, 2H, 3.74 (s, 2H), 3.73 (s, 3H).

Methyl p-nitrophenylacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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2945-08-6, Methyl p-nitrophenylacetateRelated Search:

METHYL PENTAFLUOROBENZOATE METHYL 4-AMINOSALICYLATE METHYL 3-(4-METHOXYPHENYL)PROPIONATE Methyl p-nitrophenylacetate BIS(2,4-DINITROPHENYL)ACETIC ACID ETHYL ESTER METHYL 2,4-DINITROPHENYLACETATE Ethyl 4-nitrophenylacetate ETHYL 4-NITROPHENYLGLYOXYLATE 4-Nitrophenylacetic acid 6-CHLORO-4-METHYL-3-(4'-NITROPHENYL)COUMARIN DIMETHYL 2-METHYL-2-(4-NITROPHENYL)MALONATE 2-DIETHYLAMINOETHYL 1-(4-NITROPHENYL)CYCLOPENTANECARBOXYLATE HYDROCHLORIDE methyl 2-(4-nitrophenyl)propionate 6-METHOXY-3(4'-NITROPHENYL)COUMARIN 3(4'-NITROPHENYL)COUMARIN DIMETHYL 2-(2,4-DINITROPHENYL)MALONATE 2-OXOPROPYL 2-(4-NITROPHENYL)ACETATE 5-[(DIMETHYLAMINO)METHYLENE]-4-METHYL-3-(4-NITROPHENYL)-2(5H)-FURANONE

(4-Nitrophenyl)acetic acid methyl ester

2-(p-Nitrophenyl)acetic acid methyl ester

4-Nitrobenzeneacetic acid methyl ester

4-Nitrophenylacetic acid methyl ester

Methyl 2-(4-nitrophenyl)acetate

Methyl 2-(4-nitrophenyl)

Benzeneacetic acid, 4-nitro-, methyl ester

Methyl p-nitrophenylacetate

2945-08-6