5-hydroxypipecolic acid

Product Name: 5-hydroxypipecolic acid
CAS No.: 13096-31-6
Chemical Name: 5-hydroxypipecolic acid
Synonyms: 5-hydroxy-2-piperidinecarboxylic acid;1,4,7-TRIACETATE;5-hydroxypipecolic acid;5-hydroxy piperidine-2-carboxylic acid;2-Piperidinecarboxylic acid, 5-hydroxy-
CBNumber: CB71379287
Molecular Formula: C6H11NO3
Formula Weight: 145.16
MOL File: 13096-31-6.mol

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5-hydroxypipecolic acid Property

Melting point:: 240-246 °C
Boiling point:: 354.8±42.0 °C(Predicted)
Density: 1.299±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 2.31±0.40(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0373034
Product name: 5-HYDROXYPIPERIDINE-2-CARBOXYLIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $505.1
Updated: 2021/12/16

Ambeed

Product number: A309315
Product name: 5-Hydroxypiperidine-2-carboxylicacid
Purity: 95+%
Packaging: 1g
Price: $646
Updated: 2021/12/16

Crysdot

Product number: CD11297119
Product name: 5-Hydroxypiperidine-2-carboxylicacid
Purity: 95+%
Packaging: 1g
Price: $648
Updated: 2021/12/16

Crysdot

Product number: CD11297119
Product name: 5-Hydroxypiperidine-2-carboxylicacid
Purity: 95+%
Packaging: 5g
Price: $1946
Updated: 2021/12/16

Ambeed

Product number: A309315
Product name: 5-Hydroxypiperidine-2-carboxylicacid
Purity: 95+%
Packaging: 250mg
Price: $79
Updated: 2021/12/16

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5-hydroxypipecolic acid Chemical Properties,Usage,Production

Definition

ChEBI: A piperidinemonocarboxylic acid that is pipecolic acid with a hydroxy substituent at position 5.

Synthesis

15069-92-8

13096-31-6

The general procedure for the synthesis of 5-hydroxypiperidine-2-carboxylic acid from 5-hydroxypyridine-2-carboxylic acid was as follows: compound XII (350.00 g, 2.516 mmol, 1.0 eq.) was dissolved in a solvent mixture of water (5 L) and methanol (1 L), and Pd(OH)2/C catalyst (50.00 g) was added. The mixture was transferred to an autoclave, charged with hydrogen to a pressure of 3.5 MPa, and reacted at 65°C for 24 hours. The reaction progress was monitored by LC-MS and stopped after confirming the complete disappearance of the feedstock. The reaction mixture was filtered to remove the catalyst and the filtrate was concentrated several times with toluene to give a product in the form of a brown liquid (365.22 g, aqueous solution), which was used directly in the next step of the reaction in a yield of 100% based on theoretical values.

References

[1] Patent: CN106045999, 2016, A. Location in patent: Paragraph 0068; 0069; 0070
[2] Recueil des Travaux Chimiques des Pays-Bas, 1958, vol. 77, p. 249,253

5-hydroxypipecolic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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5-hydroxypipecolic acid Suppliers

China 37 South Korea 1 United States 2 Global 40

Shanghai Topbiochem Technology Co., Ltd

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Nanjing SynTitan Pharmaceutical Co., Ltd.

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View Lastest Price from 5-hydroxypipecolic acid manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 5-hydroxypipecolic acid 13096-31-6
Price: US $3.00-9.00/KG
Min. Order: 0.1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2025-06-24

Pharmahands (Taizhou) Co., Ltd.

Product: 5-hydroxypipecolic acid 13096-31-6
Price: US $0.00-0.00/Kg/Drum
Min. Order: 1g
Purity: 99%
Supply Ability: 200kg/month
Release date: 2020-11-06

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5-hydroxypipecolic acid

5-hydroxy piperidine-2-carboxylic acid

2-Piperidinecarboxylic acid, 5-hydroxy-

5-hydroxy-2-piperidinecarboxylic acid

1,4,7-TRIACETATE

13096-31-6