ChemicalBook > CAS DataBase List > 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1

3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1

Product Name
3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1
CAS No.
1668-53-7
Chemical Name
3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1
Synonyms
DBDT;UV-107;UV-1168;Doxepin for system suitability CRS;3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-...;4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-3-benzenediol;3-benzenediol,4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl];4-[4,6-Bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1,3-Benzenediol;2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine;4-(4,6-Bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol
CBNumber
CB71453884
Molecular Formula
C25H23N3O2
Formula Weight
397.47
MOL File
1668-53-7.mol
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3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Property

Melting point:
203.0 to 207.0 °C
Boiling point:
659.1±65.0 °C(Predicted)
Density 
1?+-.0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Dimethylformamide
form 
powder to crystal
pka
8.58±0.40(Predicted)
color 
White to Light yellow to Light orange
InChI
InChI=1S/C25H23N3O2/c1-14-5-8-19(16(3)11-14)23-26-24(20-9-6-15(2)12-17(20)4)28-25(27-23)21-10-7-18(29)13-22(21)30/h5-13,29-30H,1-4H3
InChIKey
FROCQMFXPIROOK-UHFFFAOYSA-N
SMILES
C1(O)=CC=C(C2=NC(C3=CC=C(C)C=C3C)=NC(C3=CC=C(C)C=C3C)=N2)C(O)=C1
EPA Substance Registry System
1,3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]- (1668-53-7)
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Safety

HS Code 
2933.69.6050
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TCI Chemical
Product number
D4527
Product name
2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Purity
>98.0%(HPLC)(N)
Packaging
5g
Price
$103
Updated
2025/07/31
TCI Chemical
Product number
D4527
Product name
2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Purity
>98.0%(HPLC)(N)
Packaging
25g
Price
$344
Updated
2025/07/31
TRC
Product number
D458318
Product name
2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
D458318
Product name
2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Packaging
500mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD159256
Product name
2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Packaging
2g
Price
$60
Updated
2021/12/16
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3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Chemical Properties,Usage,Production

Synthesis

1237-53-2

108-46-3

1668-53-7

The general procedure for the synthesis of 4-(4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol from 2-chloro-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol using 2-chloro-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl and resorcinol was carried out as follows: in a 50 mL three-necked flask protected by a dry nitrogen gas, 2-chloro-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-1,3,5-triazin-2-yl (1.6 mmol) and 2-chloro-4,6 -bis(2,4-dimethylphenyl)-1,3,5-triazine (1.6 mmol) and anhydrous aluminum trichloride (0.32 g, 2.4 mmol) to anhydrous chlorobenzene (15 mL), and the reaction mixture was stirred for 0.5 hours at 25 °C. Subsequently, resorcinol (0.24 g, 2.2 mmol) was added and the reaction mixture was warmed up to 85 °C for continued stirring for 5 hours. Upon completion of the reaction, it was cooled to room temperature and the reaction was quenched by the slow addition of ice water (10 mL), followed by evaporation under reduced pressure to remove the chlorobenzene. The mixture was filtered and the resulting solid was washed with water (3 x 10 mL) and finally recrystallized from ethyl acetate to afford the target product 4-(4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol and its derivatives.

References

[1] Journal of Fluorescence, 2018, vol. 28, # 2, p. 707 - 723
[2] Patent: US6242598, 2001, B1

3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Suppliers

Jiangsu Nanchuang Chemical and Life Health Research Institute Co., Ltd.
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15720605021
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QQ:353175721
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China
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Shijiazhuang Yesheng Chemical Technology Co., Ltd
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18031147013 18031147013;
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0311-68030586
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yeshengchemical@163.com
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China
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TCI (Shanghai) Development Co., Ltd.
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021-67121386
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021-67121385
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Sales-CN@TCIchemicals.com
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China
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847-367-3680
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847-367-3681
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+86 (0) 571 85 58 67 18
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0086-571-85864795
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Hangzhou Yuhao Chemical Technology Co., Ltd
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Suzhou Sibian Chemical Technology Co.,Ltd.
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0512-65617459
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Nanjing Norris-Pharm Technology Co., Ltd
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+86-25-52131256
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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
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025-66113011 17798518460
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View Lastest Price from 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 manufacturers

Career Henan Chemical Co
Product
3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 1668-53-7
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2018-08-09

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