6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE

Product Name: 6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE
CAS No.: 5426-59-5
Chemical Name: 6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE
Synonyms: 6-broMo-2-Methylquinazolin-4-ol;6-bromo-2-methyl-1H-quinazolin-4-one;6-bromo-2-methyl-4(3H)-Quinazolinone;6-bromo-2-methylquinazolin-4(1H)-one;6-bromo-2-methyl-3H-quinazolin-4-one;4(3H)-Quinazolinone, 6-bromo-2-methyl-;4(1H)-Quinazolinone, 6-bromo-2-methyl-;6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE;6-bromo-2-methylquinazolin-4(3H)-one(SALTDATA: FREE)
CBNumber: CB71502674
Molecular Formula: C9H7BrN2O
Formula Weight: 239.07
MOL File: 5426-59-5.mol

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6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE Property

Melting point:: 298 °C
Boiling point:: 372.6±44.0 °C(Predicted)
Density: 1.72±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 1.96±0.20(Predicted)
Appearance: Off-white to light brown Solid

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Safety

Risk Statements: 22
Safety Statements: 36/37
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B697670
Product name: 6-Bromo-2-methylquinazolin-4(3H)-one
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B697670
Product name: 6-Bromo-2-methylquinazolin-4(3H)-one
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: B697670
Product name: 6-Bromo-2-methylquinazolin-4(3H)-one
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK231259
Product name: 6-Bromo-2-methylquinazolin-4(3H)-one
Purity: 97%
Packaging: 1g
Price: $272
Updated: 2021/12/16

Matrix Scientific

Product number: 072338
Product name: 6-Bromo-2-methylquinazolin-4(3H)-one
Purity: 95+%
Packaging: 1g
Price: $347
Updated: 2021/12/16

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6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE Chemical Properties,Usage,Production

Chemical Properties

Light yellow solid

Synthesis

108-24-7

5794-88-7

5426-59-5

The general procedure for the synthesis of 6-bromo-2-methylquinazolin-4(3H)-one from ethanoic anhydride and 2-amino-5-bromobenzoic acid was as follows: first, 2-amino-5-bromobenzoic acid was refluxed for 1 h in liquid ammonia (10 mL/g). Subsequently, the reaction solution was concentrated to a smaller volume and the residue was mixed with acetic anhydride (2 mL/g) and refluxing was continued for 4 hours. Upon completion of the reaction, water was added to the mixture and boiled for 30 minutes, followed by dropwise addition of 20% sodium hydroxide solution until a clarified solution was formed. Next, ammonium carbonate was added to the hot solution until a precipitate was formed. The mixture was allowed to stand at 4°C for 16 hours, after which the precipitate was collected by filtration, washed with water and finally dried under vacuum to give the target product in about 60% yield.

References

[1] Patent: US2009/69320, 2009, A1. Location in patent: Page/Page column 76
[2] Journal of the American Chemical Society, 1906, vol. 28, p. 101

6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE Suppliers

China 75 India 1 United States 8 Global 84

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
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Bide Pharmatech Ltd.

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Nantong MYBio-pharm. Co., Ltd.

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View Lastest Price from 6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE manufacturers

Career Henan Chemical Co

Product: 6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE 5426-59-5
Price: US $6.68/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2020-01-10

5426-59-5, 6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONERelated Search:

6-BROMO-2-METHYLIMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLIC ACID 6-BROMO-2-METHYLOXAZOLO[4,5-B]PYRIDINE 6-Bromo-2-methylimidazo[1,2-a]pyrazine 6-BROMO-2-METHYLIMIDAZO[1,2-A]PYRIDINE 6-BROMO-2-METHYL-IMIDAZO[1,2-A]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER 6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE Glycine, N-methyl-N-phenyl-, 2-(6,8-dibromo-2-methyl-4-oxo-3(4H)-quina zolinyl)ethyl ester BUTTPARK 144\07-82 beta-(6,8-Dibromo-2-methyl-3,4-dihydro-4-oxoquinazolin-3-yl)ethyl anil inoacetate 6-Bromo-2-vinyl-4-quinazolinol 6-BROMO-2-PHENYL-1H-QUINAZOLIN-4-ONE 6,8-DIBROMO-2-METHYLQUINAZOLIN-4-OL 3-amino-6-bromo-2-methylquinazolin-4(3H)-one 2-BROMO-7,8,9,10-TETRAHYDROAZEPINO[2,1-B]QUINAZOLIN-12(6H)-ONE 6-BROMO-3-HYDROXY-2-[3-(TRIFLUOROMETHYL)PHENYL]-4(3H)-QUINAZOLINONE 6-BROMO-2-(3-CHLOROPHENYL)-3-HYDROXY-4(3H)-QUINAZOLINONE 6-BROMO-2-(3,4-DICHLOROPHENYL)-3-HYDROXY-4(3H)-QUINAZOLINONE 2-Piperidinecarboxylic acid, 1-((6,8-dibromo-3,4-dihydro-4-oxo-3-pheny l-2-quinazolinyl)methyl)-

6-BROMO-2-METHYL-3,4-DIHYDROQUINAZOLIN-4-ONE

6-bromo-2-methyl-1H-quinazolin-4-one

6-bromo-2-methylquinazolin-4(3H)-one(SALTDATA: FREE)

6-broMo-2-Methylquinazolin-4-ol

6-bromo-2-methylquinazolin-4(1H)-one

6-bromo-2-methyl-4(3H)-Quinazolinone

4(1H)-Quinazolinone, 6-bromo-2-methyl-

4(3H)-Quinazolinone, 6-bromo-2-methyl-

6-bromo-2-methyl-3H-quinazolin-4-one

5426-59-5