4-BROMO-7-CHLORO-1H-INDOLE

Product Name: 4-BROMO-7-CHLORO-1H-INDOLE
CAS No.: 126811-30-1
Chemical Name: 4-BROMO-7-CHLORO-1H-INDOLE
Synonyms: 7-Chloro-5-bromoindole;4-Bromo-7-chloro-indole;7-CHLORO-4-BROMO INDOLE;4-BROMO-7-CHLORO-1H-INDOLE;1H-Indole, 4-broMo-7-chloro-;4-bromo-7-chloro-1H-indole - [B18339]
CBNumber: CB7157547
Molecular Formula: C8H5BrClN
Formula Weight: 230.49
MOL File: 126811-30-1.mol

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4-BROMO-7-CHLORO-1H-INDOLE Property

Boiling point:: 345.8±22.0 °C(Predicted)
Density: 1.772±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.49±0.30(Predicted)
Appearance: Off-white to pink Solid
InChI: InChI=1S/C8H5BrClN/c9-6-1-2-7(10)8-5(6)3-4-11-8/h1-4,11H
InChIKey: ABBUZRXDYLQKRH-UHFFFAOYSA-N
SMILES: N1C2=C(C(Br)=CC=C2Cl)C=C1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H303May be harmfulif swallowed

H320Causes eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: B702803
Product name: 4-Bromo-7-chloro-1H-indole
Packaging: 1mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B702803
Product name: 4-Bromo-7-chloro-1H-indole
Packaging: 10mg
Price: $110
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB148926
Product name: 4-Bromo-7-chloro-1H-indole
Packaging: 25mg
Price: $66
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB148926
Product name: 4-Bromo-7-chloro-1H-indole
Packaging: 50mg
Price: $114
Updated: 2021/12/16

AK Scientific

Product number: 5276AA
Product name: 4-Bromo-7-chloro-1H-indole
Packaging: 25mg
Price: $139
Updated: 2021/12/16

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4-BROMO-7-CHLORO-1H-INDOLE Chemical Properties,Usage,Production

Synthesis

16588-24-2

1826-67-1

126811-30-1

Vinylmagnesium bromide (177 mL of 1.0 M THF solution, 0.177 mol) was added slowly and dropwise to a solution of 4-bromo-1-chloro-2-nitrobenzene (14 g, 0.059 mol) dissolved in 400 mL of THF at -40 °C. The reaction mixture was stirred continuously at -40°C for 2 hours. Upon completion of the reaction, the reaction was quenched by the addition of aqueous NH4Cl, followed by extraction with ether. The organic phases were combined, dried with anhydrous Na2SO4 and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography to afford the target compound 7-chloro-4-bromoindole (6 g, 44% yield).1H NMR (CDCl3, 400 MHz) δ: 8.5 (s, 1H), 7.31-7.29 (m, 1H), 7.26-7.22 (m, 1H), 7.07-7.05 (m, 1H), 6.65-6.63 ( m, 1H).

References

[1] Patent: WO2013/117522, 2013, A1. Location in patent: Page/Page column 40
[2] Patent: US2015/18367, 2015, A1. Location in patent: Paragraph 0179; 0180
[3] Patent: KR101601357, 2016, B1. Location in patent: Paragraph 0392-0394

4-BROMO-7-CHLORO-1H-INDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-7-CHLORO-1H-INDOLE Suppliers

China 67 Ukraine 1 United Kingdom 1 United States 8 Global 77

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View Lastest Price from 4-BROMO-7-CHLORO-1H-INDOLE manufacturers

Career Henan Chemical Co

Product: 4-Bromo-7-chloro-1H-indole 126811-30-1
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1ton
Release date: 2020-01-10

126811-30-1, 4-BROMO-7-CHLORO-1H-INDOLERelated Search:

VILAZODONE 4-BROMO-7-CHLORO-1H-INDOLE 4-BROMO-7-CHLORO-1-METHYL-1H-INDOLE 4-BROMO-7-CHLORO-2-METHYL-1H-INDOLE

4-BROMO-7-CHLORO-1H-INDOLE

7-CHLORO-4-BROMO INDOLE

4-Bromo-7-chloro-indole

1H-Indole, 4-broMo-7-chloro-

7-Chloro-5-bromoindole

4-bromo-7-chloro-1H-indole - [B18339]

126811-30-1