Cyclohexanone, 4-(4-chlorophenyl)-
- Product Name
- Cyclohexanone, 4-(4-chlorophenyl)-
- CAS No.
- 14472-80-1
- Chemical Name
- Cyclohexanone, 4-(4-chlorophenyl)-
- Synonyms
- 4-(4-chlorophenyl)-;4-(p-Chlorophenyl)cyclohexanone;4-(4-chlorophenyl)cyclohexanone;4-(4-chlorophenyl)cyclohexan-1-one;4-(4-chlorophenyl)-1-cyclohexanone;Cyclohexanone, 4-(4-chlorophenyl)-
- CBNumber
- CB71872223
- Molecular Formula
- C12H13ClO
- Formula Weight
- 208.68
- MOL File
- 14472-80-1.mol
Cyclohexanone, 4-(4-chlorophenyl)- Property
- Melting point:
- 138-141 °C
- Boiling point:
- 138-141 °C(Press: 0.5 Torr)
- Density
- 1.165±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- Chloroform, Dichloromethane
- form
- Solid
- color
- White
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C377800
- Product name
- 4-(4-Chlorophenyl)cyclohexanone
- Packaging
- 50mg
- Price
- $95
- Updated
- 2021/12/16
- Product number
- C377800
- Product name
- 4-(4-Chlorophenyl)cyclohexanone
- Packaging
- 1g
- Price
- $605
- Updated
- 2021/12/16
- Product number
- FC20341
- Product name
- 4-(4-Chlorophenyl)cyclohexanone
- Packaging
- 100mg
- Price
- $40
- Updated
- 2021/12/16
- Product number
- FC20341
- Product name
- 4-(4-Chlorophenyl)cyclohexanone
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 4277CV
- Product name
- 4-(4-Chlorophenyl)cyclohexanone
- Packaging
- 250mg
- Price
- $109
- Updated
- 2021/12/16
Cyclohexanone, 4-(4-chlorophenyl)- Chemical Properties,Usage,Production
Chemical Properties
White Solid
Uses
4-(4-Chlorophenyl)cyclohexanone (cas# 14472-80-1) is a compound useful in organic synthesis.
Synthesis
1409956-58-6
14472-80-1
1409956-62-2
529-34-0
The general procedure for the synthesis of 4-(4-chlorophenyl)cyclohexanone, compound (CAS:1409956-62-2) and 1-tetrahydronaphthalenone from compound (CAS:1409956-58-6) was as follows: 2-(4-(4-chlorophenyl)-1-hydroxycyclohexyl)-3,4-dihydronaphthalen-1-(2H)-one (12.0 g, 0.034 mol) was added to a reactor equipped with an overhead stirrer and reflux condenser with a heating jacket. Toluene (200 mL) was added to suspend the feedstock, followed by the addition of p-toluenesulfonic acid (0.3 g, 2.5 mol%) to the reaction mixture. The reaction mixture was heated to 60°C and stirred for 6 h. The reaction progress was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was cooled to room temperature and the solvent was evaporated under reduced pressure to give a residue. Ethyl acetate (150 mL) was added to the residue and washed with saturated aqueous sodium bicarbonate (NaHCO3). After separation of the organic layer, the solvent was evaporated to give the crude product. The crude product was purified by recrystallization from methanol to give a white solid compound (5.3 g, 50% yield). Gas chromatographic (GC) analysis of the mother liquor obtained after recrystallization showed that α-tetralone and 4-(4-chlorophenyl)cyclohexanone were present in an approximately 1:1 ratio (based on the corresponding retention times and area percentage profiles in the mother liquor) in 50% total yield. gC retention time: α-tetralone (XII): 17.21 min (area percentage: 46).
References
[1] Patent: WO2013/14486, 2013, A1. Location in patent: Page/Page column 19
Cyclohexanone, 4-(4-chlorophenyl)- Preparation Products And Raw materials
Raw materials
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View Lastest Price from Cyclohexanone, 4-(4-chlorophenyl)- manufacturers
- Product
- Cyclohexanone, 4-(4-chlorophenyl)- 14472-80-1
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11
- Product
- Cyclohexanone, 4-(4-chlorophenyl)- 14472-80-1
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09