METHYL 3-OXOTETRADECANOATE

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METHYL 3-OXOTETRADECANOATE

Synthesis

Product Name: METHYL 3-OXOTETRADECANOATE
CAS No.: 22348-97-6
Chemical Name: METHYL 3-OXOTETRADECANOATE
Synonyms: Orlistat Impurity 61;Metyl lauroyl acetate;Methyl β-KetoMyristate;Methyl b-ketomyristate;Methyl Lauroyl Acetate;METHYL 3-OXOTETRADECANOATE;METHYL 3-KETOTETRADECANOATE;3-Oxomyristic acid methyl ester;3-Ketomyristic acid methyl ester;3-Oxotetradecanoic acid methyl ester
CBNumber: CB7187955
Molecular Formula: C15H28O3
Formula Weight: 256.38
MOL File: 22348-97-6.mol

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METHYL 3-OXOTETRADECANOATE Property

Melting point:: 29-30°C
Boiling point:: 137-139 °C(Press: 0.9 Torr)
Density: 0.926±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,2-8°C
solubility: Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form: Solid
pka: 10.65±0.46(Predicted)
color: Light Yellow to Yellow
LogP: 5.500 (est)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H413May cause long lasting harmful effects to aquatic life

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: M325865
Product name: Methyl3-Oxotetradecanoate
Packaging: 500mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 089325
Product name: Methyl 3-oxotetradecanoate
Packaging: 1g
Price: $151
Updated: 2021/12/16

Matrix Scientific

Product number: 089325
Product name: Methyl 3-oxotetradecanoate
Packaging: 5g
Price: $670
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0067306
Product name: METHYL 3-OXOTETRADECANOATE
Purity: 95.00%
Packaging: 1G
Price: $739.2
Updated: 2021/12/16

AK Scientific

Product number: Q506
Product name: Methyl3-Oxotetradecanoate
Packaging: 5g
Price: $873
Updated: 2021/12/16

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METHYL 3-OXOTETRADECANOATE Chemical Properties,Usage,Production

Synthesis

The carboxylic acid (13.8 g, 69 mmol, 1.0 equivalents) was dissolved in dry THF under an inert atmosphere and cooled to 0 ºC. CDI (13.4 g, 83 mmol, 1.2 equivalents) was then added in small portions over several minutes. After 10 min, the reaction was allowed to warm slowly to room temperature and was then stirred for 1 h. In a separate flflask, monomethyl malonate (9.8g, 83 mmol, 1.2 equivalents) was dissolved in THF under an inert atmosphere and cooled to −78 ºC. To this solution was added dibutylmagnesium (1.0 M in heptane, 0.6 equivalents). A white solid formed instantly on addition of the base. After 10 min, the reaction was warmed to room temperature and stirred for 1 h. The acylimidazole was then added by cannula to the flflask containing the magnesium salt. The resulting slurry was stirred for 3 days. The reaction mixture was then concentrated on a rotary evaporator and the residue redissolved in EtOAc. The resulting solution was washed with 1.2 M HCl, saturated aqueous NaHCO3, and brine. The organic phase was dried over sodium sulfate, fifiltered, concentrated, and the residue purifified by flflash chromatography (7:1 hexanes:EtOAc) to give the β-keto ester (14.7g, 83%).

Reference: Durham, T. B.; Miller, M. J. J. Org. Chem. 2003, 68, 27–34.

Chemical Properties

Yellow Crystalline Solid

Uses

Methyl 3-Oxotetradecanoate (cas# 22348-97-6) is a compound useful in organic synthesis.

METHYL 3-OXOTETRADECANOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from METHYL 3-OXOTETRADECANOATE manufacturers

Career Henan Chemical Co

Product: METHYL 3-OXOTETRADECANOATE 22348-97-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%HPLC
Supply Ability: 10t
Release date: 2019-12-24

22348-97-6, METHYL 3-OXOTETRADECANOATERelated Search:

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METHYL 3-OXOTETRADECANOATE

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