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3-BROMOPHENANTHRENE

Product Name
3-BROMOPHENANTHRENE
CAS No.
715-50-4
Chemical Name
3-BROMOPHENANTHRENE
Synonyms
3-BROMOPHENTHRENE;3-BROMOPHENANTHRENE;Phenanthrene, 3-bromo-;3-Bromophenanthrene >3-Bromophenanthrene 96%;3-Bromophenanthrene in isooctane
CBNumber
CB7206014
Molecular Formula
C14H9Br
Formula Weight
257.13
MOL File
715-50-4.mol
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3-BROMOPHENANTHRENE Property

Melting point:
81-86 °C
Boiling point:
389.7±11.0 °C(Predicted)
Density 
1.479±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
powder to crystal
color 
White to Orange to Green
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Safety

Hazard Codes 
Xi
Risk Statements 
20/21/22-50/53-41-37/38
Safety Statements 
22-36/37/39-61-60-39-26
RIDADR 
UN 3077 9 / PGIII
WGK Germany 
3
HS Code 
2903998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
748323
Product name
3-Bromophenanthrene
Purity
96%
Packaging
250mg
Price
$91.8
Updated
2024/03/01
TCI Chemical
Product number
B2387
Product name
3-Bromophenanthrene
Purity
>98.0%(GC)
Packaging
100mg
Price
$302
Updated
2024/03/01
TRC
Product number
B678858
Product name
3-Bromophenanthrene
Packaging
1mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
X4431
Product name
3-Bromophenanthrene
Packaging
250mg
Price
$145
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB58935
Product name
3-bromophenanthrene
Packaging
25mg
Price
$200
Updated
2021/12/16
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3-BROMOPHENANTHRENE Chemical Properties,Usage,Production

Uses

3-Bromophenanthrene can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.

Synthesis


3 -bromophenanthreneTo a 250 mL vessel equipped with a pyrex inner water-cooled jacket was added l-bromo-4-[2- phenylvinyl] benzene (520 mg, 2.0 mmol) from Step 1 above, in cyclohexane (230 mL) and THF (5 mL). To this solution was added iodine (770 mg, 3.0 mmol). The stirred solution was first degassed by bubbling nitrogen and was then exposed to UV light for 16 hours by inserting a 450 W medium pressure mercury lamp in the inner insert. The reaction was quenched with 10% Na2S2?3 and the aqueous layer was extracted with ethyl acetate. The combined organic layers were washed with brine, dried over Na2SO4 and the volatiles were removed under reduced pressure. The crude material was purified by flash chromatography on silica (100 % hexanes) to afford 3-bromophenanthrene (486 mg, 94%) as a white solid.

3-BROMOPHENANTHRENE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-BROMOPHENANTHRENE Suppliers

TOKYO CHEMICAL INDUSTRY CO., LTD.
Tel
03-36680489
Fax
03-3668-0520
Email
Sales-JP@TCIchemicals.com
Country
Japan
ProdList
28387
Advantage
80
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View Lastest Price from 3-BROMOPHENANTHRENE manufacturers

Speranza Chemical Co., Ltd.
Product
3-Bromophenanthrene 715-50-4
Price
US $2500.00/KG
Min. Order
1KG
Purity
98%+
Supply Ability
300MT/year
Release date
2019-12-24
Henan Fengda Chemical Co., Ltd
Product
3-Bromophenanthrene 715-50-4
Price
US $200.00-1.00/KG
Min. Order
1KG
Purity
99%, 99.5% Sublimated
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-31
Henan Aochuang Chemical Co.,Ltd.
Product
3-BROMOPHENANTHRENE 715-50-4
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-09-27