Uses
ChemicalBook > CAS DataBase List > 2,6-Dichloronicotinamide

2,6-Dichloronicotinamide

Uses
Product Name
2,6-Dichloronicotinamide
CAS No.
62068-78-4
Chemical Name
2,6-Dichloronicotinamide
Synonyms
DichloronicotinaMide;2,6-Dichloronicotimide;Nicotinamide Impurity 99;2,6-Dichloronicotinamide;2,6-Dichloropyridine-3-carboxamide;3-Pyridinecarboxamide, 2,6-dichloro-;2,6-Dichloropyridine-3-carboxamide 97%;2,6-Dichloronicotinamide ISO 9001:2015 REACH
CBNumber
CB72100659
Molecular Formula
C6H4Cl2N2O
Formula Weight
191.01
MOL File
62068-78-4.mol
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2,6-Dichloronicotinamide Property

Melting point:
148-151 °C
Boiling point:
315.5±42.0 °C(Predicted)
Density 
1.524±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
powder
pka
13.91±0.50(Predicted)
Appearance
White to off-white Solid
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Safety

Hazard Codes 
Xn
Risk Statements 
22-36/37/38
Safety Statements 
26
WGK Germany 
3
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
702145
Product name
2,6-Dichloropyridine-3-carboxamide
Purity
97%
Packaging
5g
Price
$334
Updated
2023/06/20
Sigma-Aldrich
Product number
702145
Product name
2,6-Dichloropyridine-3-carboxamide
Purity
97%
Packaging
1g
Price
$76
Updated
2023/01/07
TRC
Product number
D435738
Product name
2,6-Dichloronicotinamide
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
D435738
Product name
2,6-Dichloronicotinamide
Packaging
50mg
Price
$60
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0066583
Product name
2,6-DICHLOROPYRIDINE-3-CARBOXAMIDE
Purity
95.00%
Packaging
25G
Price
$1501.5
Updated
2021/12/16
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2,6-Dichloronicotinamide Chemical Properties,Usage,Production

Uses

2,6-Dichloronicotinamide is used as a research compound and in organic synthesis, etc.

Synthesis

40381-90-6

62068-78-4

General procedure for the synthesis of 2,6-dichloronicotinamide from 2,6-dichloronicotinonitrile: To 2,6-dichloronicotinonitrile (1.73 g, 10 mmol) was added concentrated sulfuric acid (10 mL) and water (2 mL). The reaction mixture was heated to 90 °C and stirred continuously for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently slowly poured into ice water. The pH of the mixture was adjusted with ammonia to 8. The precipitate precipitated was collected by filtration, washed with cold water (20 mL) and finally dried under vacuum to give 2,6-dichloronicotinamide as a brown solid (1.4 g, 73% yield). Mass spectrum (ESI): m/z = 191.1 [M + H]+.

References

[1] Patent: WO2015/48662, 2015, A2. Location in patent: Page/Page column 37
[2] Patent: CN107226805, 2017, A. Location in patent: Paragraph 0097; 0098; 0099; 0100; 0101

2,6-Dichloronicotinamide Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-Dichloronicotinamide Suppliers

INTATRADE GmbH
Tel
+49 3493/605464
Fax
+49 3493/605470
Email
sales@intatrade.de
Country
Germany
ProdList
3572
Advantage
66
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
Advantage
61
JinYan Chemicals(ShangHai) Co.,Ltd.
Tel
13817811078
Fax
86-021-50426522,50426273
Email
sales@jingyan-chemical.com
Country
China
ProdList
9976
Advantage
60
Changzhou Huanling Chemical Co., Ltd.
Tel
0519-89803565 13776850645
Fax
0519-89803575
Email
info4@huanlingchem.com
Country
China
ProdList
891
Advantage
68
Shandong Xiya Chemical Co., Ltd
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18729
Advantage
57
Syntechem Co.,Ltd
Tel
Fax
E-Mail Inquiry
Email
info@syntechem.com
Country
China
ProdList
12984
Advantage
57
Beijing Yisiyan Technology Research Center
Tel
010-56645598 13366904824
Fax
01062230033
Email
bjkaida@163.com
Country
China
ProdList
1618
Advantage
59
Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66113011 17798518460
Fax
(1)02557626880
Email
cfzhang@aikonchem.com
Country
China
ProdList
19913
Advantage
55
JIANGYIN CANAL PHARMTECH CO.,LIMITED.
Tel
+86-18921203887
Fax
+86-0510-86319635 ; QQ:1622023101
Email
sales@canalpharm.net
Country
China
ProdList
288
Advantage
58
Shanghai Hong-chuang Pharma Tech Co., Ltd.
Tel
18151128828
Fax
-
Email
hc-sales@foxmail.com
Country
China
ProdList
2647
Advantage
55
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View Lastest Price from 2,6-Dichloronicotinamide manufacturers

Career Henan Chemical Co
Product
2,6-Dichloronicotinamide 62068-78-4
Price
US $1.00/kg
Min. Order
1g
Purity
99%
Supply Ability
100KG
Release date
2018-12-21

62068-78-4, 2,6-DichloronicotinamideRelated Search:


  • 2,6-Dichloronicotinamide
  • 2,6-Dichloropyridine-3-carboxamide
  • DichloronicotinaMide
  • 2,6-Dichloronicotimide
  • 2,6-Dichloropyridine-3-carboxamide 97%
  • 3-Pyridinecarboxamide, 2,6-dichloro-
  • 2,6-Dichloronicotinamide ISO 9001:2015 REACH
  • Nicotinamide Impurity 99
  • 62068-78-4