2,6-Dichloronicotinamide
Uses- Product Name
- 2,6-Dichloronicotinamide
- CAS No.
- 62068-78-4
- Chemical Name
- 2,6-Dichloronicotinamide
- Synonyms
- DichloronicotinaMide;2,6-Dichloronicotimide;Nicotinamide Impurity 99;2,6-Dichloronicotinamide;2,6-Dichloropyridine-3-carboxamide;3-Pyridinecarboxamide, 2,6-dichloro-;2,6-Dichloropyridine-3-carboxamide 97%;2,6-Dichloronicotinamide ISO 9001:2015 REACH
- CBNumber
- CB72100659
- Molecular Formula
- C6H4Cl2N2O
- Formula Weight
- 191.01
- MOL File
- 62068-78-4.mol
2,6-Dichloronicotinamide Property
- Melting point:
- 148-151 °C
- Boiling point:
- 315.5±42.0 °C(Predicted)
- Density
- 1.524±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- powder
- pka
- 13.91±0.50(Predicted)
- Appearance
- White to off-white Solid
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-36/37/38
- Safety Statements
- 26
- WGK Germany
- 3
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 702145
- Product name
- 2,6-Dichloropyridine-3-carboxamide
- Purity
- 97%
- Packaging
- 5g
- Price
- $334
- Updated
- 2023/06/20
- Product number
- 702145
- Product name
- 2,6-Dichloropyridine-3-carboxamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $76
- Updated
- 2023/01/07
- Product number
- D435738
- Product name
- 2,6-Dichloronicotinamide
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D435738
- Product name
- 2,6-Dichloronicotinamide
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- HCH0066583
- Product name
- 2,6-DICHLOROPYRIDINE-3-CARBOXAMIDE
- Purity
- 95.00%
- Packaging
- 25G
- Price
- $1501.5
- Updated
- 2021/12/16
2,6-Dichloronicotinamide Chemical Properties,Usage,Production
Uses
2,6-Dichloronicotinamide is used as a research compound and in organic synthesis, etc.
Synthesis
40381-90-6
62068-78-4
General procedure for the synthesis of 2,6-dichloronicotinamide from 2,6-dichloronicotinonitrile: To 2,6-dichloronicotinonitrile (1.73 g, 10 mmol) was added concentrated sulfuric acid (10 mL) and water (2 mL). The reaction mixture was heated to 90 °C and stirred continuously for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently slowly poured into ice water. The pH of the mixture was adjusted with ammonia to 8. The precipitate precipitated was collected by filtration, washed with cold water (20 mL) and finally dried under vacuum to give 2,6-dichloronicotinamide as a brown solid (1.4 g, 73% yield). Mass spectrum (ESI): m/z = 191.1 [M + H]+.
References
[1] Patent: WO2015/48662, 2015, A2. Location in patent: Page/Page column 37
[2] Patent: CN107226805, 2017, A. Location in patent: Paragraph 0097; 0098; 0099; 0100; 0101
2,6-Dichloronicotinamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,6-Dichloronicotinamide manufacturers
- Product
- 2,6-Dichloronicotinamide 62068-78-4
- Price
- US $1.00/kg
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-12-21