2-Chloro-3-nitropyridine-6-amine
- Product Name
- 2-Chloro-3-nitropyridine-6-amine
- CAS No.
- 84487-03-6
- Chemical Name
- 2-Chloro-3-nitropyridine-6-amine
- Synonyms
- 6-Chloro-5-nitropyridin-2-aMine;6-Chloro-5-nitro-2-pyridinamine;2-Amino-6-chloro-5-nitropyridine;2-Chloro-6-amino-3-nitropyridine;6-Amino-2-chloro-3-nitropyridine;2-Chloro-3-nitropyridine-6-amine;2-Pyridinamine, 6-chloro-5-nitro-;6-Chloro-5-nitro-pyridin-2-ylaMine;2-Chloro-3-nitropyridine-6-amine 98%min;2-Chloro-3-nitropyridine-6-amine ISO 9001：2015 REACH
- CBNumber
- CB72266946
- Molecular Formula
- C5H4ClN3O2
- Formula Weight
- 173.56
- MOL File
- 84487-03-6.mol
2-Chloro-3-nitropyridine-6-amine Property
- Melting point:
- 188 °C
- Boiling point:
- 393.6±37.0 °C(Predicted)
- Density
- 1.596±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- -1.22±0.37(Predicted)
- Appearance
- Yellow to green Solid
N-Bromosuccinimide Price
- Product number
- C611385
- Product name
- 6-chloro-5-nitropyridin-2-amine
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C611385
- Product name
- 6-chloro-5-nitropyridin-2-amine
- Packaging
- 100mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- FC141550
- Product name
- 6-Chloro-5-nitropyridin-2-amine
- Packaging
- 100mg
- Price
- $70
- Updated
- 2021/12/16
- Product number
- FC141550
- Product name
- 6-Chloro-5-nitropyridin-2-amine
- Packaging
- 250mg
- Price
- $140
- Updated
- 2021/12/16
- Product number
- W8714
- Product name
- 6-Chloro-5-nitropyridin-2-amine
- Packaging
- 250mg
- Price
- $150
- Updated
- 2021/12/16
2-Chloro-3-nitropyridine-6-amine Chemical Properties,Usage,Production
Synthesis
45644-21-1
84487-03-6
The general procedure for the synthesis of 2-amino-5-nitro-6-chloropyridine from 2-amino-6-chloropyridine was as follows: concentrated nitric acid (2.39 mL, 35.00 mmol) was slowly added dropwise at 0 °C to a mixture containing concentrated sulfuric acid (56 mL, 1050 mmol) and 6-chloropyridin-2-amine (3.00 g, 23.34 mmol). The reaction mixture was kept stirred at 0 °C for 4 hours. After completion of the reaction, the mixture was carefully poured into ice water. The mixture was extracted with ethyl acetate (3 x 100 mL). The organic layers were combined, dried with anhydrous sodium sulfate and subsequently concentrated. The residue was purified by column chromatography to afford the target product 2-amino-5-nitro-6-chloropyridine (1.38 g, 34% yield).
References
[1] Patent: WO2018/146472, 2018, A1. Location in patent: Page/Page column 54; 55
[2] Patent: WO2018/146469, 2018, A1. Location in patent: Page/Page column 44-45
2-Chloro-3-nitropyridine-6-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Chloro-3-nitropyridine-6-amine manufacturers
- Product
- 2-Chloro-3-nitropyridine-6-amine 84487-03-6
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-09-07