2-(3-Aminophenyl)acetic acid ethyl ester
- Product Name
- 2-(3-Aminophenyl)acetic acid ethyl ester
- CAS No.
- 52273-79-7
- Chemical Name
- 2-(3-Aminophenyl)acetic acid ethyl ester
- Synonyms
- Ethyl 2-(3-aminophenyl)acetate;Ethyl 3-aminophenylacetate;3-Amino-benzeneacetic acid ethyl ester;(3-Aminophenyl)acetic acid ethyl ester;2-(3-Aminophenyl)acetic acid ethyl ester;Benzeneacetic acid, 3-amino-, ethyl ester
- CBNumber
- CB72347678
- Molecular Formula
- C10H13NO2
- Formula Weight
- 179.22
- MOL File
- 52273-79-7.mol
2-(3-Aminophenyl)acetic acid ethyl ester Property
- Boiling point:
- 138-140 °C(Press: 3-4 Torr)
- Density
- 1.112±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 4.36±0.10(Predicted)
- Appearance
- Brown to black Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- E937453
- Product name
- Ethyl2-(3-Aminophenyl)acetate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CHM0398976
- Product name
- ETHYL-2-(3-AMINOPHENYL)ACETATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.15
- Updated
- 2021/12/16
- Product number
- CD12065363
- Product name
- Ethyl2-(3-aminophenyl)acetate
- Purity
- 95+%
- Packaging
- 25g
- Price
- $634
- Updated
- 2021/12/16
- Product number
- A-5958
- Product name
- 3-Amino-benzeneaceticacidethylester
- Purity
- 97%
- Packaging
- 0.5g
- Price
- $73.33
- Updated
- 2021/12/16
- Product number
- A-5958
- Product name
- 3-Amino-benzeneaceticacidethylester
- Purity
- 97%
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
2-(3-Aminophenyl)acetic acid ethyl ester Chemical Properties,Usage,Production
Synthesis
14318-64-0
52273-79-7
General procedure for the synthesis of ethyl 2-(3-aminophenyl)acetate from ethyl 3-nitrophenylacetate: ethyl 2-(3-nitrophenyl)acetate (3h) (1.05 g, 3.40 mmol) was dissolved in methanol (25 mL) and hydrogenation reaction was carried out for 4 h by adding 10% Pd/C (catalytic amount) as a catalyst. After completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated to afford the target product ethyl 2-(3-aminophenyl)acetate (4h). The product was characterized by 1H-NMR (200 MHz, CDCl3): δ 1.25 (t, 3H, J = 7.2 Hz), 3.51 (s, 2H), 4.14 (q, 2H, J = 7.2 Hz), 6.59-6.71 (m, 3H), 7.11 (t, 1H, J = 7.8 Hz). The reaction was carried out quantitatively in 100% yield.
References
[1] Patent: EP3381898, 2018, A1. Location in patent: Paragraph 0200; 0265
[2] Collection of Czechoslovak Chemical Communications, 1995, vol. 60, # 4, p. 659 - 669
[3] Bioorganic and Medicinal Chemistry, 2008, vol. 16, # 3, p. 1206 - 1217
[4] Bioorganic and Medicinal Chemistry Letters, 2005, vol. 15, # 1, p. 217 - 220
[5] Patent: US6150373, 2000, A
2-(3-Aminophenyl)acetic acid ethyl ester Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(3-Aminophenyl)acetic acid ethyl ester manufacturers
- Product
- 2-(3-Aminophenyl)acetic acid ethyl ester 52273-79-7
- Price
- US $65.00-650.00/kg
- Min. Order
- 10kg
- Purity
- 0.99
- Supply Ability
- 20tons
- Release date
- 2023-11-09