7-METHOXY-2-METHYLQUINOLINE
- Product Name
- 7-METHOXY-2-METHYLQUINOLINE
- CAS No.
- 19490-87-0
- Chemical Name
- 7-METHOXY-2-METHYLQUINOLINE
- Synonyms
- 2-Methyl-7-Methoxyquinoline;7-METHOXY-2-METHYLQUINOLINE;Quinoline, 7-methoxy-2-methyl-
- CBNumber
- CB72450747
- Molecular Formula
- C11H11NO
- Formula Weight
- 173.21
- MOL File
- 19490-87-0.mol
7-METHOXY-2-METHYLQUINOLINE Property
- Boiling point:
- 286.0±20.0 °C(Predicted)
- Density
- 1.102±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 6.15±0.50(Predicted)
- Appearance
- Colorless to light yellow Liquid
N-Bromosuccinimide Price
- Product number
- BBO000218
- Product name
- 7-Methoxy-2-methylquinoline
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $332
- Updated
- 2023/01/07
- Product number
- M341710
- Product name
- 7-Methoxy-2-methylquinoline
- Packaging
- 500mg
- Price
- $285
- Updated
- 2021/12/16
- Product number
- 0084AB
- Product name
- 7-Methoxy-2-methylquinoline
- Packaging
- 5g
- Price
- $1615
- Updated
- 2021/12/16
- Product number
- 4H56-1-549
- Product name
- 7-Methoxy-2-methylquinoline
- Packaging
- 1g
- Price
- $456
- Updated
- 2021/12/16
- Product number
- 19490870
- Product name
- 7-Methoxy-2-methylquinoline
- Packaging
- 5g
- Price
- $1051.66
- Updated
- 2021/12/16
7-METHOXY-2-METHYLQUINOLINE Chemical Properties,Usage,Production
Synthesis
64-17-5
536-90-3
19490-87-0
General procedure for the synthesis of 2-methyl-7-methoxyquinoline from ethanol and m-aminoanisole: 0.005 mmol (1.1 mg) of transition metal catalyst was accurately weighed and placed in a 10 mL Young reaction tube equipped with a magnetic stirrer. Under oxygen atmosphere, 0.04 mmol of co-catalyst I, 0.08 mmol of co-catalyst II, 0.2 mmol of 3-methoxyaniline and 1 mL of anhydrous ethanol were added sequentially to the reaction tube. The reaction mixture was stirred at 150 °C for 16 hours. After completion of the reaction, the pH of the reaction solution was adjusted to neutral and left to stand for subsequent processing. The target product 2-methyl-7-methoxyquinoline was purified by column chromatography in 88% yield.
References
[1] Patent: CN106543078, 2017, A. Location in patent: Paragraph 0089; 0090
[2] Tetrahedron Letters, 2010, vol. 51, # 37, p. 4911 - 4914
[3] Research on Chemical Intermediates, 2012, vol. 38, # 3-5, p. 761 - 773
[4] Journal of Organic Chemistry, 2017, vol. 82, # 6, p. 3284 - 3290
[5] Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013, vol. 43, # 4, p. 500 - 508
7-METHOXY-2-METHYLQUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
7-METHOXY-2-METHYLQUINOLINE Suppliers
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