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3,3-DIMETHYLAZETIDINE HYDROCHLORIDE

Product Name
3,3-DIMETHYLAZETIDINE HYDROCHLORIDE
CAS No.
89381-03-3
Chemical Name
3,3-DIMETHYLAZETIDINE HYDROCHLORIDE
Synonyms
1101-4;3,3-DIMETHYLAZETIDINE HCL;3,3-DIMETHYLAZETIDINE HYDROCHLORIDE;Azetidine, 3,3-dimethyl-, hydrochloride (1:1);3,3-Dimethylazetidine hydrochloride - [D11454]
CBNumber
CB72453980
Molecular Formula
C5H12ClN
Formula Weight
121.61
MOL File
89381-03-3.mol
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3,3-DIMETHYLAZETIDINE HYDROCHLORIDE Property

Melting point:
96-98 °C
storage temp. 
Inert atmosphere,Room Temperature
form 
solid
color 
Pale yellow
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC
Product number
B401843
Product name
3,3-dimethylazetidinehydrochloride
Packaging
100mg
Price
$65
Updated
2021/12/16
TRC
Product number
B401843
Product name
3,3-dimethylazetidinehydrochloride
Packaging
500mg
Price
$265
Updated
2021/12/16
AK Scientific
Product number
5732AJ
Product name
3,3-Dimethylazetidinehydrochloride
Packaging
1g
Price
$267
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD146346
Product name
3,3-Dimethylazetidine hydrochloride
Packaging
500mg
Price
$350
Updated
2021/12/16
Matrix Scientific
Product number
113028
Product name
3,3-Dimethylazetidine hydrochloride
Packaging
1g
Price
$473
Updated
2021/12/16
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3,3-DIMETHYLAZETIDINE HYDROCHLORIDE Chemical Properties,Usage,Production

Chemical Properties

colourless liquid

Synthesis

79201-18-6

89381-03-3

Compounds 1-6 (7.2 g, 30 mmol) were used as starting materials and dissolved in 100 mL of n-pentanol. The temperature of the reaction system was maintained at 110 °C and 6.9 g of sodium metal was added in batches. After the sodium metal was completely reacted, the reaction was continued with stirring for 1 hour, followed by cooling to room temperature. 100mL of water was added to the reaction mixture and the aqueous phase was separated. The organic phase was washed three times with 450mL of 2N hydrochloric acid solution. The solvent was removed by rotary evaporator and the resulting residue was dissolved in 100 mL of aqueous 2N NaOH solution and subsequently extracted three times with 300 mL of dichloromethane. The organic phases were combined, washed twice with saturated aqueous sodium chloride solution and dried with anhydrous sodium sulfate. To the dried organic phase was added 100 mL of 2N hydrochloric acid, and the solvent was removed by concentration via rotary evaporation to give the final target product 3,3-dimethylazetidine hydrochloride (Compounds 1-7, 0.9 g, 24.7% yield) as a white solid.

References

[1] Patent: EP2738156, 2014, A1. Location in patent: Paragraph 0090-0091

3,3-DIMETHYLAZETIDINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3,3-DIMETHYLAZETIDINE HYDROCHLORIDE Suppliers

China 73 India 2 United Kingdom 2 United States 5 Global 82
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 3,3-DIMETHYLAZETIDINE HYDROCHLORIDE manufacturers

Career Henan Chemical Co
Product
3,3-DIMETHYLAZETIDINE HYDROCHLORIDE 89381-03-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2020-01-09

89381-03-3, 3,3-DIMETHYLAZETIDINE HYDROCHLORIDERelated Search:

Zetidoline 1-(2-CHLOROPYRIDIN-3-YL)-3,3-DIMETHYLAZETIDIN-2-ONE EZETIMIBE ANALOGUE 1-(3-CHLORO-2-METHYLPHENYL)-3,3-DIMETHYL-2-AZETANONE 1-(5-CHLORO-2-PYRIDINYL)-3,3-DIMETHYL-2-AZETANONE 3,3-DIMETHYL-1-(2,4,6-TRICHLOROANILINO)-2-AZETANONE 1-(4-[1-(4-CHLOROPHENYL)-1H-PYRAZOL-5-YL]PHENYL)-3,3-DIMETHYL-2-AZETANONE 1-(3-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]OXY)PHENYL)-3,3-DIMETHYL-2-AZETANONE 3-[4-(3,3-DIMETHYL-2-OXO-1-AZETANYL)PHENYL]-3-OXOPROPANAL O-(2-CHLORO-6-FLUOROBENZYL)OXIME 3-[4-(3,3-DIMETHYL-2-OXO-1-AZETANYL)PHENYL]-3-OXOPROPANAL O-(4-CHLOROBENZYL)OXIME 1-(2,4-DICHLOROPHENYL)-3,3-DIMETHYL-2-AZETANONE 1-(2-BENZOYL-4-CHLOROPHENYL)-3,3-DIMETHYL-2-AZETANONE 3-([(2-CHLORO-4-FLUOROBENZYL)OXY]IMINO)-2-[4-(3,3-DIMETHYL-2-OXO-1-AZETANYL)PHENYL]PROPANENITRILE 1-(4-[3-(4-CHLOROPHENYL)PYRAZOLO[1,5-A]PYRIMIDIN-7-YL]PHENYL)-3,3-DIMETHYL-2-AZETANONE 1-[[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL](METHYL)AMINO]-3,3-DIMETHYL-2-AZETANONE 1-(4-(2-[(3-CHLOROBENZYL)SULFANYL][1,2,4]TRIAZOLO[1,5-A]PYRIMIDIN-7-YL)PHENYL)-3,3-DIMETHYL-2-AZETANONE 1-(3,5-DICHLOROPHENYL)-3,3-DIMETHYL-2-AZETANONE N-(([(2-CHLORO-4-FLUOROBENZYL)OXY]IMINO)METHYL)-2-(3,3-DIMETHYL-2-OXO-1-AZETANYL)-3-PHENYLPROPANAMIDE

  • 3,3-DIMETHYLAZETIDINE HYDROCHLORIDE
  • 3,3-DIMETHYLAZETIDINE HCL
  • 1101-4
  • Azetidine, 3,3-dimethyl-, hydrochloride (1:1)
  • 3,3-Dimethylazetidine hydrochloride - [D11454]
  • 89381-03-3
  • 89351-03-3