DI(1H-IMIDAZOL-1-YL)METHANIMINE
- Product Name
- DI(1H-IMIDAZOL-1-YL)METHANIMINE
- CAS No.
- 104619-51-4
- Chemical Name
- DI(1H-IMIDAZOL-1-YL)METHANIMINE
- Synonyms
- EOS-60817;Di(1-iMidazolyl)MethaniMine;Di (1H imidazol-1-yl) imine;di(imidazol-1-yl)methanimine;Di(1H-imidazol-2-yl)methanimine;DI(1H-IMIDAZOL-1-YL)METHANIMINE;Di (1 hydrogen imidazolyl) imine;C,C-di(imidazol-1-yl)methaneimine;1,1'-Carbonimidoylbis-1H-imidazole;1,1'-Carbonimidoylbis[1H-imidazole
- CBNumber
- CB72454846
- Molecular Formula
- C7H7N5
- Formula Weight
- 161.16
- MOL File
- 104619-51-4.mol
DI(1H-IMIDAZOL-1-YL)METHANIMINE Property
- Melting point:
- 103-104℃
- Boiling point:
- 355℃
- Density
- 1.38
- Flash point:
- 169℃
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- pka
- 4.19±0.70(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C7H7N5/c8-7(11-3-1-9-5-11)12-4-2-10-6-12/h1-6,8H
- InChIKey
- FKGQRXQOODICAT-UHFFFAOYSA-N
- SMILES
- C(N1C=NC=C1)(N1C=NC=C1)=N
Safety
- HS Code
- 2933299090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- D476993
- Product name
- Di(1H-imidazol-1-yl)methanimine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FC45505
- Product name
- 1,1'-Carbonimidoylbis-1H-imidazole
- Packaging
- 2g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- OR917034
- Product name
- 1,1'-Carbonimidoylbis-1H-imidazole
- Purity
- 95%
- Packaging
- 1g
- Price
- $155
- Updated
- 2021/12/16
- Product number
- CS-D0450
- Product name
- 1,1'-Carbonimidoylbis[1H-imidazole]
- Packaging
- 5g
- Price
- $184
- Updated
- 2021/12/16
- Product number
- CS-D0450
- Product name
- 1,1'-Carbonimidoylbis[1H-imidazole]
- Packaging
- 1g
- Price
- $55
- Updated
- 2021/12/16
DI(1H-IMIDAZOL-1-YL)METHANIMINE Chemical Properties,Usage,Production
Synthesis
288-32-4
506-68-3
104619-51-4
Cyanogen bromide (22.5 g, 212 mmol) was slowly added to a solution of 1H-imidazole (42 g, 617 mmol) in dichloromethane (1 L) and the reaction mixture was heated to reflux for 30 min. After completion of the reaction, it was cooled to room temperature and white solid was observed to precipitate. The solid was separated by filtration. The filtrate was concentrated under reduced pressure to about 100 mL and subsequently allowed to stand in a refrigerator for 3 days to promote crystallization. The precipitated solid was collected by filtration to give the final bis(1H-imidazol-1-yl)methanimine (8 g, 49.6 mmol, 8% yield).
References
[1] Patent: US2012/149718, 2012, A1. Location in patent: Page/Page column 35
[2] Journal of Organic Chemistry, 2002, vol. 67, # 21, p. 7553 - 7556
[3] Journal of Heterocyclic Chemistry, 2003, vol. 40, # 1, p. 191 - 193
[4] Chemical Communications, 2014, vol. 50, # 91, p. 14257 - 14260
[5] Patent: WO2012/85586, 2012, A1. Location in patent: Page/Page column 66; 68
DI(1H-IMIDAZOL-1-YL)METHANIMINE Preparation Products And Raw materials
Raw materials
Preparation Products
DI(1H-IMIDAZOL-1-YL)METHANIMINE Suppliers
- Tel
- --
- Fax
- --
- sales@carbosynth.com
- Country
- United Kingdom
- ProdList
- 6005
- Advantage
- 58
View Lastest Price from DI(1H-IMIDAZOL-1-YL)METHANIMINE manufacturers
- Product
- DI(1H-IMIDAZOL-1-YL)METHANIMINE 104619-51-4
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- customise
- Release date
- 2018-08-09