5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE

Product Name: 5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE
CAS No.: 566158-47-2
Chemical Name: 5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE
Synonyms: 5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE;4-(5-Bromo-3-methyl-2-pyridyl)morpholine;Morpholine, 4-(5-broMo-3-Methyl-2-pyridinyl)-
CBNumber: CB72455959
Molecular Formula: C10H13BrN2O
Formula Weight: 257.13
MOL File: 566158-47-2.mol

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5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE Property

Density: 1.441
storage temp.: 2-8°C

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB154348
Product name: 5-Bromo-3-methyl-2-(morpholino)pyridine
Packaging: 100mg
Price: $85
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB154348
Product name: 5-Bromo-3-methyl-2-(morpholino)pyridine
Packaging: 250mg
Price: $170
Updated: 2021/12/16

Matrix Scientific

Product number: 052107
Product name: 4-(5-Bromo-3-methyl-2-pyridinyl)morpholine
Packaging: 500mg
Price: $237
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB154348
Product name: 5-Bromo-3-methyl-2-(morpholino)pyridine
Packaging: 500mg
Price: $295
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB154348
Product name: 5-Bromo-3-methyl-2-(morpholino)pyridine
Packaging: 1g
Price: $511
Updated: 2021/12/16

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5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE Chemical Properties,Usage,Production

Synthesis

110-91-8

29312-98-9

566158-47-2

K2CO3 (5.5 g, 39.6 mmol) was added as 5-bromo-2-fluoro-3-methylpyridine (2.5 g, 13.2 mmol) and morpholine (3.4 g, 39.2 mmol) dissolved in 40 mL of DMSO. The reaction mixture was heated to 120 °C and stirred for 16 hours. After the reaction was completed, the mixture was cooled to room temperature. 200 mL of water was added to the reaction mixture and extracted with ethyl acetate (150 mL x 3). The organic layers were combined, washed sequentially with 150 mL of water and 150 mL of brine, and dried with anhydrous Na2SO4. The organic layer was concentrated under reduced pressure to afford the target compound 5-bromo-3-methyl-2-(morpholinato)pyridine (1.8 g, 53% yield) as a white solid.LC-MS detection: [M + H]+ = 257.0.

References

[1] Patent: US2016/176882, 2016, A1. Location in patent: Paragraph 0427; 0428
[2] Patent: WO2017/221100, 2017, A1. Location in patent: Paragraph 00217

5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE Suppliers

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566158-47-2, 5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINERelated Search:

methyl 5-bromo-2-morpholinonicotinate 4-(5-BROMOPYRIDIN-2-YL)MORPHOLINE 5-BROMO-4,6-DIMETHYL-2-MORPHOLINONICOTINONITRILE 5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE

5-BROMO-3-METHYL-2-(MORPHOLINO)PYRIDINE

Morpholine, 4-(5-broMo-3-Methyl-2-pyridinyl)-

4-(5-Bromo-3-methyl-2-pyridyl)morpholine

566158-47-2

Heterocycle-Pyridine series