6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE
Uses- Product Name
- 6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE
- CAS No.
- 914947-26-5
- Chemical Name
- 6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE
- Synonyms
- 6-BROMO-2-PYRIDINEMETHANAMINEHCLSALT;(6-BROMOPYRIDIN-2-YL)METHANAMINE HCL;6-bromo-2-pyridinemethanamine hydrochL;6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE;(6-Bromo-2-pyridyl)methanamine hydrochloride;C-(6-Bromo-pyridin-2-yl)-methylamine dihydrochloride
- CBNumber
- CB72459982
- Molecular Formula
- C6H8BrClN2
- Formula Weight
- 223.5
- MOL File
- 914947-26-5.mol
6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- FB150846
- Product name
- 6-Bromo-2-pyridinemethanamine,hydrochloride
- Packaging
- 100mg
- Price
- $68
- Updated
- 2021/12/16
- Product number
- 215138
- Product name
- (6-Bromopyridin-2-yl)methanaminehydrochloride
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $104
- Updated
- 2021/12/16
- Product number
- FB150846
- Product name
- 6-Bromo-2-pyridinemethanamine,hydrochloride
- Packaging
- 250mg
- Price
- $135
- Updated
- 2021/12/16
- Product number
- 215138
- Product name
- (6-Bromopyridin-2-yl)methanaminehydrochloride
- Purity
- 95+%
- Packaging
- 1g
- Price
- $207
- Updated
- 2021/12/16
- Product number
- 118023
- Product name
- (6-Bromopyridin-2-yl)methanamine hydrochloride
- Packaging
- 1g
- Price
- $226
- Updated
- 2021/12/16
6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE Chemical Properties,Usage,Production
Uses
6-Bromo-2-pyridinemethylamine hydrochloride is the form of 6-bromo-2-pyridinemethylamine hydrochloride. 6-Bromo-2-pyridinemethylamine is an important organic intermediate that can be prepared from 2-bromo-6-hydroxymethylpyridine and can be used in laboratory research and development processes as well as in chemical and pharmaceutical synthesis processes.
Synthesis
2- [(6-Bromopyridin-2-yl)methyl]-2,3-dihydro-1H-isoindole-1,3-dione (2.5 g, 7.88 mmol, 1.0 eq.) was dissolved in anhydrous ethanol (78 mL) in a 250 mL round-bottomed flask fitted with a magnetic stirring bar and a condenser and heated to reflux until completely dissolved (~15 min). Hydrazine monohydrate (1.58 g, 1.53 mL, 31.53 mmol, 4.0 eq.) was added to the homogeneous solution. Within one minute, the reaction mixture turned yellow. The reaction mixture was heated for 3 hours, during which time the mixture solidified into a white thick suspension. Another 50 mL of ethanol was added and the mixture was stirred for another 2 hours. The reaction was cooled to room temperature and then to 0 C to precipitate the hydrazine/phthalimide adduct that disintegrated in solution. The precipitate was filtered over a Buchner. The precipitate was washed well with anhydrous ethanol and the filtrate was partially concentrated. Some solids remained in the suspension, which was then filtered with cold EtOH. The filtrate was concentrated to dryness to give a solid.
6-BROMO-2-PYRIDINEMETHANAMINE, HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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