ChemicalBook > CAS DataBase List > (R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE

(R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE

Product Name: (R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE
CAS No.: 474707-30-7
Chemical Name: (R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE
Synonyms: (R)-3-Methoxypyrrolidine HCl;(3R)-3-Methoxy-pyrrolidine HCl;(R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE;(3R)-3-METHOXYPYRROLIDINE HYDROCHLORIDE;(3R)-3-Methoxypyrrolidine hydrochloride (1:1);Pyrrolidine, 3-methoxy-, hydrochloride (1:1), (3R)-
CBNumber: CB72465417
Molecular Formula: C5H12ClNO
Formula Weight: 137.61
MOL File: 474707-30-7.mol

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(R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: light brown solid
InChI: InChI=1/C5H11NO.ClH/c1-7-5-2-3-6-4-5;/h5-6H,2-4H2,1H3;1H/t5-;/s3
InChIKey: SQMYKVUSWPIFEQ-USHJBNIQNA-N
SMILES: O([C@H]1CNCC1)C.Cl |&1:1,r|

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M333033
Product name: (R)-3-MethoxypyrrolidineHydrochloride
Packaging: 500mg
Price: $175
Updated: 2021/12/16

Matrix Scientific

Product number: 112127
Product name: ((R)-3-Methoxypyrrolidine hydrochloride
Packaging: 1g
Price: $189
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-5-R3
Product name: (3R)-3-Methoxypyrrolidine hydrochloride
Packaging: 1g
Price: $150
Updated: 2021/12/16

Activate Scientific

Product number: AS12327-B
Product name: (R)-3-Methoxypyrrolidine HCl
Purity: 95+% ee
Packaging: 1g
Price: $157
Updated: 2021/12/16

Ark Pharm

Product number: P000106028
Product name: (R)-3-Methoxypyrrolidine hydrochloride
Purity: 95%
Packaging: 250mg
Price: $33
Updated: 2021/12/16

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(R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

549532-08-3

474707-30-7

The general procedure for the synthesis of (R)-3-methoxypyrrolidine hydrochloride from (R)-N-Boc-3-methoxytetrahydropyrrole was as follows: tert-butyl (R)-3-methoxypyrrolidine-1-carboxylate (1100 mg, 5.47 mmol) was dissolved in 4M HCl/dioxane solution (15 mL, 60 mmol), and the reaction was stirred for 16 hours at 20 °C. After completion of the reaction, the reaction mixture was concentrated to give the crude product (1000 mg, 7.27 mmol) as an oil. The structure of the product was confirmed by 1H NMR (CDCl3, 400 MHz) with the following chemical shifts: δH= 10.10-9.39 (m, 2H), 4.13-4.04 (m, 1H), 3.51-3.35 (m, 4H), 3.31 (s, 3H), 2.24-2.12 (m, 1H), 2.08-1.95 (m, 1H) .

References

[1] Patent: WO2005/49616, 2005, A1. Location in patent: Page/Page column 79
[2] Patent: WO2005/97799, 2005, A1. Location in patent: Page/Page column 125-126
[3] Patent: WO2004/37809, 2004, A1. Location in patent: Page 50
[4] Patent: WO2018/148745, 2018, A1. Location in patent: Page/Page column 168

(R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE manufacturers

Career Henan Chemical Co

Product: (R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE 474707-30-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 500kg/month
Release date: 2019-08-01

474707-30-7, (R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDERelated Search:

(3R)-3-METHOXYPYRROLIDINE HYDROCHLORIDE

(R)-3-METHOXY-PYRROLIDINE HYDROCHLORIDE

(R)-3-Methoxypyrrolidine HCl

(3R)-3-Methoxypyrrolidine hydrochloride (1:1)

Pyrrolidine, 3-methoxy-, hydrochloride (1:1), (3R)-

(3R)-3-Methoxy-pyrrolidine HCl

474707-30-7