ChemicalBook > CAS DataBase List > 2,5,6-trichloronicotinaMide

2,5,6-trichloronicotinaMide

Product Name: 2,5,6-trichloronicotinaMide
CAS No.: 142266-62-4
Chemical Name: 2,5,6-trichloronicotinaMide
Synonyms: 2,5,6-trichloronicotinaMide;2,5,6-Trichloro-nicotineamide;2,5,6-Trichloropyridin-3-carboxamide;2,5,6-Trichloro-3-pyridinecarboxaMide;2,5,6-trichloropyridine-3-carboxamide;3-Pyridinecarboxamide, 2,5,6-trichloro-
CBNumber: CB72549443
Molecular Formula: C6H3Cl3N2O
Formula Weight: 225.46
MOL File: 142266-62-4.mol

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2,5,6-trichloronicotinaMide Property

Boiling point:: 290.0±40.0 °C(Predicted)
Density: 1.643±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 13.32±0.50(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 6947AA
Product name: 2,5,6-Trichloronicotinamide
Packaging: 100mg
Price: $201
Updated: 2021/12/16

AK Scientific

Product number: 6947AA
Product name: 2,5,6-Trichloronicotinamide
Packaging: 250mg
Price: $257
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0362797
Product name: 2,5,6-TRICHLORONICOTINAMIDE
Purity: 95.00%
Packaging: 5MG
Price: $500.89
Updated: 2021/12/16

Matrix Scientific

Product number: 179556
Product name: 2,5,6-Trichloronicotinamide
Packaging: 1g
Price: $826
Updated: 2021/12/16

Matrix Scientific

Product number: 179556
Product name: 2,5,6-Trichloronicotinamide
Packaging: 5g
Price: $1650
Updated: 2021/12/16

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2,5,6-trichloronicotinaMide Chemical Properties,Usage,Production

Synthesis

58584-88-6

142266-62-4

General procedure for the synthesis of 2,5,6-trichloropyridin-3-amide from 2,5,6-trichloronicotinoyl chloride: a solution of dioxane (20 ml) of 2,5,6-trichloronicotinoyl chloride (2.5 g, 10.2 mmol) was slowly added dropwise to 10 ml of ammonium hydroxide (28% NH3 aqueous solution) at 0 °C. After the dropwise addition, the reaction mixture was continued to be stirred at 0°C for 10 min. Subsequently, extraction was carried out with dichloromethane (3 x 50 ml). All organic phases were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford 2,5,6-trichloropyridin-3-amide (2.3 g, 100% yield), which could be used in subsequent reactions without further purification.

References

[1] Patent: WO2006/82392, 2006, A1. Location in patent: Page/Page column 109
[2] Bioorganic and Medicinal Chemistry, 2002, vol. 10, # 6, p. 1793 - 1804
[3] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 10, p. 2958 - 2961

2,5,6-trichloronicotinaMide Preparation Products And Raw materials

Raw materials

Preparation Products

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142266-62-4, 2,5,6-trichloronicotinaMideRelated Search:

2,5,6-trichloronicotinaMide

2,5,6-Trichloro-3-pyridinecarboxaMide

3-Pyridinecarboxamide, 2,5,6-trichloro-

2,5,6-trichloropyridine-3-carboxamide

2,5,6-Trichloro-nicotineamide

2,5,6-Trichloropyridin-3-carboxamide

142266-62-4