10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

Product Name: 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
CAS No.: 4014-77-1
Chemical Name: 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
Synonyms: Licarbazepine Impurity 5;Oxcarbazepine Impurity 27;10,11-dihydro-5H-dibenzo[b,f]azepin-10-o;10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol;5H-Dibenz[b,f]azepin-10-ol, 10,11-dihydro-;6,11-dihydro-5H-benzo[b][1]benzazepin-5-ol
CBNumber: CB72604465
Molecular Formula: C14H13NO
Formula Weight: 211.26
MOL File: 4014-77-1.mol

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D458523
Product name: 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol
Packaging: 100mg
Price: $330
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD141318
Product name: 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol
Packaging: 500mg
Price: $390
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD141318
Product name: 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD141318
Product name: 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol
Packaging: 100mg
Price: $113
Updated: 2021/12/16

AK Scientific

Product number: J54021
Product name: 10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol
Packaging: 1g
Price: $495
Updated: 2021/12/16

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10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Chemical Properties,Usage,Production

Synthesis

21737-58-6

4014-77-1

The general procedure for the synthesis of 10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol from 5H-dibenzo[b,f]azepin-10(11H)-one was as follows: 5H-dibenzo[b,f]azepin-10(11H)-one (350.0 g, 1.67 mol) was suspended in water (0.7 L) and methanol (2.8 L) in a mixed solvents. Sodium borohydride (76 g, 2.0 mol) was added in batches over 10 min without cooling and the reaction mixture was stirred continuously at 45 °C for 1 h. The reaction was completed by the addition of acetone (1.0 g, 2.0 mol). Upon completion of the reaction, acetone (350 mL) was added cautiously to quench the reaction and the reaction mixture was subsequently concentrated to a smaller volume. The target product was precipitated by the addition of water (700 mL) and the precipitate was collected and dried at 60-65 °C to afford (S)-10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol (315 g, 89.0% yield) as an off-white solid with a purity of >98%.

References

[1] Tetrahedron Letters, 2013, vol. 54, # 22, p. 2841 - 2844

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o Preparation Products And Raw materials

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Preparation Products

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View Lastest Price from 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o 4014-77-1
Price: US $1.00-2.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100000KG
Release date: 2024-07-26

4014-77-1, 10,11-dihydro-5H-dibenzo[b,f]azepin-10-oRelated Search:

10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

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4014-77-1