Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-

Product Name: Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
CAS No.: 23428-77-5
Chemical Name: Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
Synonyms: 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone;1-(4-methoxy-3-phenylmethoxyphenyl)ethanone;1-(3-(benzyloxy)-4-methoxyphenyl)ethan-1-one;Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
CBNumber: CB72614680
Molecular Formula: C16H16O3
Formula Weight: 256.3
MOL File: 23428-77-5.mol

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Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Property

Melting point:: 76 °C
Boiling point:: 396.5±27.0 °C(Predicted)
Density: 1.115±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Powder

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: Y2092
Product name: 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
Packaging: 250mg
Price: $158
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0386724
Product name: 1-(3-(BENZYLOXY)-4-METHOXYPHENYL)ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $497.21
Updated: 2021/12/16

AK Scientific

Product number: Y2092
Product name: 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
Packaging: 5g
Price: $1117
Updated: 2021/12/16

Ambeed

Product number: A121844
Product name: 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
Purity: 95+%
Packaging: 100mg
Price: $63
Updated: 2021/12/16

Ambeed

Product number: A121844
Product name: 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
Purity: 95+%
Packaging: 250mg
Price: $84
Updated: 2021/12/16

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Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Chemical Properties,Usage,Production

Synthesis

6100-74-9

100-39-0

23428-77-5

In a 200 mL round bottom flask, 4-methoxy-3-hydroxyacetophenone (4.66 g, 28.1 mmol, 1.0 eq.) and potassium carbonate (3.89 g, 28.1 mmol, 1.0 eq.) were added and dissolved in 50 mL of acetone. After stirring for 30 minutes at room temperature, benzyl bromide (5 mL, 29.4 mmol, 1.0 eq.) was slowly added. The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the mixture was cooled to room temperature, diluted with 150 mL of pure water, and then extracted with chloroform (100 mL x 4). The organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated. The concentrate was recrystallized with 3 mL of ethyl acetate, filtered and dried under vacuum to obtain the first batch of crystals. The mother liquor was further concentrated, recrystallized with 0.5 mL of ethyl acetate, filtered and dried in vacuum to obtain the second batch of crystals. Coral-like crystals of 1-(3-(benzyloxy)-4-methoxyphenyl)ethanone (compound IV1) were finally obtained, yield: 6.69 g (26.1 mmol, 93% yield).

References

[1] Patent: JP2015/214531, 2015, A. Location in patent: Paragraph 0188; 0189; 0190
[2] Bulletin of the Chemical Society of Japan, 2016, vol. 89, # 1, p. 125 - 134
[3] Beilstein Journal of Organic Chemistry, 2015, vol. 11, p. 884 - 892
[4] Journal of Heterocyclic Chemistry, 2018, vol. 55, # 3, p. 670 - 684
[5] Phytochemistry (Elsevier), 1991, vol. 30, # 7, p. 2438 - 2439

Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Suppliers

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View Lastest Price from Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone 23428-77-5
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-10

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23428-77-5