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6-BroMo-N1-Methylbenzene-1,2-diaMine

Product Name
6-BroMo-N1-Methylbenzene-1,2-diaMine
CAS No.
1150102-47-8
Chemical Name
6-BroMo-N1-Methylbenzene-1,2-diaMine
Synonyms
6-Bromo-N1-methylbenzene-1,2-diamin;6-Bromo-N1-methyl-1,2-benzenediamine;3-bromo-N2-methyl-1,2-benzenediamine;6-BroMo-N1-Methylbenzene-1,2-diaMine;3-bromo-2-N-methylbenzene-1,2-diamine;1,2-Benzenediamine, 3-bromo-N2-methyl-;3-Bromo-N*2*-methyl-benzene-1,2-diamine
CBNumber
CB72735879
Molecular Formula
C7H9BrN2
Formula Weight
201.06
MOL File
1150102-47-8.mol
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6-BroMo-N1-Methylbenzene-1,2-diaMine Property

Boiling point:
297.9±30.0 °C(Predicted)
Density 
1.578±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
5.48±0.11(Predicted)
InChI
InChI=1S/C7H9BrN2/c1-10-7-5(8)3-2-4-6(7)9/h2-4,10H,9H2,1H3
InChIKey
BVQOQXXITQULGQ-UHFFFAOYSA-N
SMILES
C1(N)=CC=CC(Br)=C1NC
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H319Causes serious eye irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B111530
Product name
6-Bromo-N1-methylbenzene-1,2-diamine
Packaging
10mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-0116339
Product name
6-Bromo-N1-methylbenzene-1,2-diamine
Purity
96.03%
Packaging
5g
Price
$847
Updated
2021/12/16
ChemScene
Product number
CS-0116339
Product name
6-Bromo-N1-methylbenzene-1,2-diamine
Purity
96.03%
Packaging
250mg
Price
$90
Updated
2021/12/16
ChemScene
Product number
CS-0116339
Product name
6-Bromo-N1-methylbenzene-1,2-diamine
Purity
96.03%
Packaging
1g
Price
$227
Updated
2021/12/16
Ambeed
Product number
A207266
Product name
6-Bromo-N1-methylbenzene-1,2-diamine
Purity
97%
Packaging
1g
Price
$235
Updated
2021/12/16
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6-BroMo-N1-Methylbenzene-1,2-diaMine Chemical Properties,Usage,Production

Synthesis

1004618-77-2

1150102-47-8

General procedure for the synthesis of 6-bromo-N1-methylbenzene-1,2-diamine from 2-bromo-N-methyl-6-nitroaniline: a mixture of the product of the previous step, 2-bromo-N-methyl-6-nitroaniline (8 g, 34.62 mmol, 1.00 eq.), with zinc powder (4 g, 62.50 mmol, 2.00 eq.) in acetic acid (120 mL) was reacted at room temperature The reaction was stirred for 16 hours at room temperature. After completion of the reaction, the insoluble solids were removed by filtration and the filtrate was concentrated under vacuum. The concentrated residue was dissolved in dichloromethane (300 mL), washed with saturated sodium bicarbonate solution (100 mL), and the organic phase was dried with anhydrous sodium sulfate and concentrated again under vacuum to give the target product 6-bromo-N1-methylbenzene-1,2-diamine (4 g, 57% yield) as a black oil.LC-MS (electrospray ionization, m/z): 201.

References

[1] Patent: US2018/162822, 2018, A1. Location in patent: Paragraph 0557
[2] Patent: WO2009/58728, 2009, A1. Location in patent: Page/Page column 73
[3] Patent: WO2008/12623, 2008, A1. Location in patent: Page/Page column 62
[4] Patent: WO2017/223229, 2017, A1. Location in patent: Paragraph 00515; 00516

6-BroMo-N1-Methylbenzene-1,2-diaMine Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BroMo-N1-Methylbenzene-1,2-diaMine Suppliers

China 49 India 1 United States 4 Global 54
Accela ChemBio Inc.
Tel
+1-858-6993322
Fax
(+1)-858-876-1948
Email
info@accelachem.com
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United States
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21193
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58
Aladdin Scientific
Tel
Email
tp@aladdinsci.com
Country
United States
ProdList
52923
Advantage
58
Synthonix Inc
Tel
--
Fax
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Email
info@synthonix.com
Country
United States
ProdList
6872
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Combi-Blocks Inc.
Tel
--
Fax
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Email
sales@combi-blocks.com
Country
United States
ProdList
6618
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View Lastest Price from 6-BroMo-N1-Methylbenzene-1,2-diaMine manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
6-BroMo-N1-Methylbenzene-1,2-diaMine 1150102-47-8
Price
US $0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1000kg
Release date
2025-05-16

1150102-47-8, 6-BroMo-N1-Methylbenzene-1,2-diaMineRelated Search:


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  • 3-bromo-N2-methyl-1,2-benzenediamine
  • 1,2-Benzenediamine, 3-bromo-N2-methyl-
  • 3-bromo-2-N-methylbenzene-1,2-diamine
  • 6-Bromo-N1-methylbenzene-1,2-diamin
  • 6-Bromo-N1-methyl-1,2-benzenediamine
  • 1150102-47-8