3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
- Product Name
- 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
- CAS No.
- 550364-01-7
- Chemical Name
- 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
- Synonyms
- 3-(1H-1,2,3-triazol-5-yl)benzonitrile;3-(2H-1,2,3-Triazol-4-yl)benzonitrile;3-(1H-(1,2,3)Triazol-4-yl)-benzonitrile;Benzonitrile, 3-(1H-1,2,3-triazol-5-yl)-;3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
- CBNumber
- CB7390285
- Molecular Formula
- C9H6N4
- Formula Weight
- 170.17
- MOL File
- 550364-01-7.mol
3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- V0804
- Product name
- 3-(1H-(1,2,3)Triazol-4-yl)-benzonitrile
- Packaging
- 250mg
- Price
- $235
- Updated
- 2021/12/16
- Product number
- CHM0379077
- Product name
- 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE-3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.07
- Updated
- 2021/12/16
- Product number
- 126343
- Product name
- 3-(2H-1,2,3-Triazol-4-yl)benzonitrile
- Purity
- >95%
- Packaging
- 1g
- Price
- $1224
- Updated
- 2021/12/16
- Product number
- 550364017
- Product name
- 3-(2H-1,2,3-Triazol-4-yl)benzonitrile
- Packaging
- 250mg
- Price
- $230.86
- Updated
- 2021/12/16
- Product number
- 550364017
- Product name
- 3-(2H-1,2,3-Triazol-4-yl)benzonitrile
- Packaging
- 1g
- Price
- $612.85
- Updated
- 2021/12/16
3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Chemical Properties,Usage,Production
Synthesis
62248-92-4
550364-01-7
To a 25 mL Schlenk tube fitted with a magnetic stirrer were sequentially added nitroolefins (0.2 mmol), sodium azide (0.3 mmol), N,N-dimethylformamide (2 mL) and Amberlyst-15 (30 mg). After sealing the reaction tube, the reaction was stirred at 50°C under air atmosphere for 1-3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC), and when the reaction was complete, the reaction mixture was extracted with ethyl acetate (3 x 10 mL). The organic phases were combined, dried over anhydrous sodium sulfate and filtered, and concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by silica gel column chromatography (petroleum ether-ethyl acetate system) to afford the target compound 3-(1H-(1,2,3)triazol-4-yl)-benzonitrile.
References
[1] Synthesis (Germany), 2016, vol. 48, # 1, p. 131 - 135
3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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