3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE

Product Name: 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
CAS No.: 550364-01-7
Chemical Name: 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
Synonyms: 3-(1H-1,2,3-triazol-5-yl)benzonitrile;3-(2H-1,2,3-Triazol-4-yl)benzonitrile;3-(1H-(1,2,3)Triazol-4-yl)-benzonitrile;Benzonitrile, 3-(1H-1,2,3-triazol-5-yl)-;3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
CBNumber: CB7390285
Molecular Formula: C9H6N4
Formula Weight: 170.17
MOL File: 550364-01-7.mol

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3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: V0804
Product name: 3-(1H-(1,2,3)Triazol-4-yl)-benzonitrile
Packaging: 250mg
Price: $235
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0379077
Product name: 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE-3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE
Purity: 95.00%
Packaging: 5MG
Price: $496.07
Updated: 2021/12/16

Matrix Scientific

Product number: 126343
Product name: 3-(2H-1,2,3-Triazol-4-yl)benzonitrile
Purity: >95%
Packaging: 1g
Price: $1224
Updated: 2021/12/16

Alichem

Product number: 550364017
Product name: 3-(2H-1,2,3-Triazol-4-yl)benzonitrile
Packaging: 250mg
Price: $230.86
Updated: 2021/12/16

Alichem

Product number: 550364017
Product name: 3-(2H-1,2,3-Triazol-4-yl)benzonitrile
Packaging: 1g
Price: $612.85
Updated: 2021/12/16

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3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Chemical Properties,Usage,Production

Synthesis

62248-92-4

550364-01-7

To a 25 mL Schlenk tube fitted with a magnetic stirrer were sequentially added nitroolefins (0.2 mmol), sodium azide (0.3 mmol), N,N-dimethylformamide (2 mL) and Amberlyst-15 (30 mg). After sealing the reaction tube, the reaction was stirred at 50°C under air atmosphere for 1-3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC), and when the reaction was complete, the reaction mixture was extracted with ethyl acetate (3 x 10 mL). The organic phases were combined, dried over anhydrous sodium sulfate and filtered, and concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by silica gel column chromatography (petroleum ether-ethyl acetate system) to afford the target compound 3-(1H-(1,2,3)triazol-4-yl)-benzonitrile.

References

[1] Synthesis (Germany), 2016, vol. 48, # 1, p. 131 - 135

3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE Suppliers

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550364-01-7, 3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILERelated Search:

3-(1H-1,2,3-TRIAZOL-4-YL)BENZONITRILE AND 3-(2H-1,2,3-TRIAZOL-4-YL)BENZONITRILE

3-(1H-(1,2,3)Triazol-4-yl)-benzonitrile

3-(2H-1,2,3-Triazol-4-yl)benzonitrile

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3-(1H-1,2,3-triazol-5-yl)benzonitrile

550364-01-7