Methyl 5-methoxy-1H-indole-3-carboxylate

Product Name: Methyl 5-methoxy-1H-indole-3-carboxylate
CAS No.: 172595-68-5
Chemical Name: Methyl 5-methoxy-1H-indole-3-carboxylate
Synonyms: RARECHEM AL BF 0096;Methyl 5-Methoxy-indole-3-carboxylate;METHYL 5-METHOXY-1H-INDOLE-3-CARBOXYLATE;methyl 5-methoxy-1H-indole-3-carboxylic acid;5-METHOXY-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER;5-Methoxyl-1H-3-Indole-carboxylicacid,, Methyl ester;1H-Indole-3-carboxylic acid, 5-methoxy-, methyl ester
CBNumber: CB7393428
Molecular Formula: C11H11NO3
Formula Weight: 205.21
MOL File: 172595-68-5.mol

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Methyl 5-methoxy-1H-indole-3-carboxylate Property

storage temp.: Sealed in dry,Room Temperature
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M338593
Product name: Methyl5-Methoxy-1H-indole-3-carboxylate
Packaging: 500mg
Price: $200
Updated: 2021/12/16

AK Scientific

Product number: W3765
Product name: Methyl5-methoxy-1H-indole-3-carboxylate
Packaging: 5g
Price: $290
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 36165
Product name: Methyl5-methoxy-1H-indole-3-carboxylate
Purity: 95+%
Packaging: 250mg
Price: $400
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0094327
Product name: 1H-INDOLE-3-CARBOXYLIC ACID,5-METHOXY-,METHYL ESTER
Purity: 95.00%
Packaging: 2G
Price: $1674.75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0094327
Product name: 1H-INDOLE-3-CARBOXYLIC ACID,5-METHOXY-,METHYL ESTER
Purity: 95.00%
Packaging: 5G
Price: $2607.41
Updated: 2021/12/16

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Methyl 5-methoxy-1H-indole-3-carboxylate Chemical Properties,Usage,Production

Uses

Methyl 5-methoxy-1H-indole-3-carboxylate is a useful reactant for the synthesis of tetrahydropyridoindoles via ruthenium-catalyzed decarboxylative C-H alkenylation .

Synthesis

7424-91-1

19501-58-7

172595-68-5

The general procedure for the synthesis of methyl 5-methoxy-1H-indole-3-carboxylate from methyl 3,3-dimethoxypropionate and 4-methoxyphenylhydrazine hydrochloride was as follows (Intermediate Example 38): 4-methoxyphenylhydrazine hydrochloride (200 mg) and methyl 3,3-dimethoxypropionate (194 mg) were added to acetic acid (8.0 mL). The reaction mixture was stirred at 70 °C for 4.5 hours. After completion of the reaction, the solvent was removed by concentration under reduced pressure and the residue was purified by column chromatography (eluent: ethyl acetate/hexane, 1:5→1:3) to afford the target product methyl 5-methoxy-1H-indole-3-carboxylate (259 mg, yield: 97%). The product was characterized by 1H NMR (DMSO-d6): δ 3.8 (3H, s), 3.9 (3H, s), 6.8 (1H, dd), 7.4 (1H, d), 7.5 (1H, d), 8.0 (1H, s), 11.8 (1H, brs).ESI/MS (m/z): 204 ([M-H]-).

References

[1] Patent: EP1595866, 2005, A1. Location in patent: Page/Page column 18

Methyl 5-methoxy-1H-indole-3-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 5-methoxy-1H-indole-3-carboxylate Suppliers

Canada 1 China 48 Germany 1 India 2 United Kingdom 1 United States 10 Global 63

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View Lastest Price from Methyl 5-methoxy-1H-indole-3-carboxylate manufacturers

Career Henan Chemical Co

Product: Methyl 5-methoxy-1H-indole-3-carboxylate 172595-68-5
Price: US $0.01/KG
Min. Order: 1KG
Purity: 98%; 99%
Supply Ability: 1kg; 10kg; 25kg
Release date: 2020-01-07

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METHYL 5-METHOXY-1H-INDOLE-3-CARBOXYLATE

5-METHOXY-1H-INDOLE-3-CARBOXYLIC ACID METHYL ESTER

RARECHEM AL BF 0096

1H-Indole-3-carboxylic acid, 5-methoxy-, methyl ester

methyl 5-methoxy-1H-indole-3-carboxylic acid

Methyl 5-Methoxy-indole-3-carboxylate

5-Methoxyl-1H-3-Indole-carboxylicacid,, Methyl ester

172595-68-5

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