3-PHENYL-PYRIDIN-2-YLAMINE
- Product Name
- 3-PHENYL-PYRIDIN-2-YLAMINE
- CAS No.
- 87109-10-2
- Chemical Name
- 3-PHENYL-PYRIDIN-2-YLAMINE
- Synonyms
- 3-PHENYL-2-PYRIDINAMINE;3-Phenyl-2-pyridylaMine;2-AMINO-3-PHENYLPYRIDINE;2-PyridinaMine,3-phenyl-;3-PHENYL-PYRIDIN-2-YLAMINE
- CBNumber
- CB7453142
- Molecular Formula
- C11H10N2
- Formula Weight
- 170.21
- MOL File
- 87109-10-2.mol
3-PHENYL-PYRIDIN-2-YLAMINE Property
- Boiling point:
- 320.3±22.0 °C(Predicted)
- Density
- 1.133
- storage temp.
- 2-8°C(protect from light)
- pka
- 6.29±0.36(Predicted)
- Appearance
- White to light yellow Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B522723
- Product name
- 3-phenylpyridin-2-amine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CHM0008425
- Product name
- 2-AMINO-3-PHENYLPYRIDINE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $1106.49
- Updated
- 2021/12/16
- Product number
- 072958
- Product name
- 3-Phenylpyridin-2-ylamine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $745
- Updated
- 2021/12/16
- Product number
- W8939
- Product name
- 3-Phenylpyridin-2-ylamine
- Packaging
- 250mg
- Price
- $184
- Updated
- 2021/12/16
- Product number
- 3H30-1-TB
- Product name
- 3-Phenylpyridin-2-ylamine
- Purity
- 95%
- Packaging
- 250mg
- Price
- $208
- Updated
- 2021/12/16
3-PHENYL-PYRIDIN-2-YLAMINE Chemical Properties,Usage,Production
Synthesis
13534-99-1
98-80-6
87109-10-2
General procedure for the synthesis of 2-amino-3-phenylpyridine from 2-amino-3-bromopyridine and phenylboronic acid: to a solution of 2-amino-3-bromopyridine (3 mmol, 0.5 g) in ethylene glycol (5 mL) was added phenylboronic acid (4.5 or 9.0 mmol, 1.5 or 3 eq.), tetrakis(triphenylphosphine)palladium(0) (1 mol%) and potassium phosphate (6 mmol, 6 eq.) in sequence. 2 eq.) in water (2 mL). The reaction mixture was heated at 80 °C for 16 h. After completion of the reaction, it was hydrolyzed with 1 M sodium hydroxide solution (20 mL). The aqueous phase was extracted with ethyl acetate (3 x 30 mL) and the combined organic layers were washed with saturated sodium chloride solution (50 mL), dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The residue was purified by silica gel column chromatography using petroleum ether/ethyl acetate (60/40, v/v) as eluent.
References
[1] Chemistry - A European Journal, 2013, vol. 19, # 28, p. 9137 - 9141
[2] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 1, p. 114 - 120
[3] Bioorganic and Medicinal Chemistry Letters, 2017, vol. 27, # 4, p. 911 - 917
[4] Patent: WO2011/17342, 2011, A2. Location in patent: Page/Page column 116
[5] Patent: WO2015/148344, 2015, A2. Location in patent: Page/Page column 60
3-PHENYL-PYRIDIN-2-YLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-PHENYL-PYRIDIN-2-YLAMINE manufacturers
- Product
- 3-PHENYL-PYRIDIN-2-YLAMINE 87109-10-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98% HPLC
- Supply Ability
- 10 tons
- Release date
- 2020-03-04