ChemicalBook > CAS DataBase List > BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE

BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE

Product Name: BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE
CAS No.: 147269-67-8
Chemical Name: BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE
Synonyms: 3-(Cbz-amino)pyridin-2(1H)-one;benzyl 2-hydroxypyridin-3-ylcarbaMate;benzyl N-(2-oxo-1H-pyridin-3-yl)carbamate;BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE;benzyl N-(2-oxo-1,2-dihydropyridin-3-yl)carbaMate;2-Oxo-1,2-dihydropyridine-3-carbamic acid benzyl ester;(2-Oxo-1,2-dihydropyridin-3-yl)carbamic acid benzyl ester;BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE ISO 9001：2015 REACH;Carbamic acid, N-(1,2-dihydro-2-oxo-3-pyridinyl)-, phenylmethyl ester
CBNumber: CB7474190
Molecular Formula: C13H12N2O3
Formula Weight: 244.25
MOL File: 147269-67-8.mol

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BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE Property

Melting point:: 175-178 °C
Boiling point:: 474.3±45.0 °C(Predicted)
Density: 1.29±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 8.52±0.20(Predicted)
Appearance: Off-white to pink Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: W3212
Product name: Benzyl(2-oxo-1,2-dihydropyridin-3-yl)carbamate
Packaging: 250mg
Price: $131
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0362271
Product name: BENZYL-2-OXO-1,2-DIHYDROPYRIDIN-3-YL-CARBAMATE
Purity: 95.00%
Packaging: 5MG
Price: $503.2
Updated: 2021/12/16

Chemenu

Product number: CM122377
Product name: benzyl(2-oxo-1,2-dihydropyridin-3-yl)carbamate
Purity: 95%
Packaging: 1g
Price: $179
Updated: 2021/12/16

Chemenu

Product number: CM122377
Product name: benzyl(2-oxo-1,2-dihydropyridin-3-yl)carbamate
Purity: 95%
Packaging: 5g
Price: $655
Updated: 2021/12/16

Crysdot

Product number: CD11252547
Product name: Benzyl(2-oxo-1,2-dihydropyridin-3-yl)carbamate
Purity: 95+%
Packaging: 5g
Price: $693
Updated: 2021/12/16

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BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE Chemical Properties,Usage,Production

Synthesis

33630-99-8

501-53-1

147269-67-8

At room temperature, 3-aminopyridin-2(1H)-one (3.25 g, 29.5 mmol) and sodium carbonate (6.26 g, 59.0 mmol) were dissolved in tetrahydrofuran (100 mL), and benzyl chloroformate (5.27 mL, 36.9 mmol) was added slowly and dropwise. The reaction mixture was stirred at room temperature for 24 hours. Upon completion of the reaction, the reaction mixture was diluted with ethyl acetate (150 mL) and filtered through Celite. The filtrate was concentrated under reduced pressure to about 200 mL and subsequently washed with water (40 mL) and dried with anhydrous magnesium sulfate. It was again concentrated under reduced pressure to about 50 mL and the precipitated white solid (first product) was collected by filtration. The remaining filtrate was concentrated to near dryness under reduced pressure and the residue was stirred with ether (50 mL) and the insoluble white solid (second batch of product) was collected by diafiltration. The two batches of products were combined and dried under vacuum at 50 °C to afford the target compound (2-oxo-1,2-dihydropyridin-3-yl)carbamic acid benzyl ester (5.77 g, 23.62 mmol, 80% yield) as a white solid.

References

[1] ChemMedChem, 2011, vol. 6, # 7, p. 1228 - 1237
[2] Patent: WO2007/27729, 2007, A1. Location in patent: Page/Page column 39-40
[3] Patent: WO2015/89143, 2015, A1. Location in patent: Page/Page column 83; 84
[4] Journal of Medicinal Chemistry, 1994, vol. 37, # 19, p. 3090 - 3099
[5] Patent: US2007/287696, 2007, A1. Location in patent: Page/Page column 33

BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE 147269-67-8
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-13

NewCan Biotech Limited

Product: Benzyl (2-oxo-1,2-dihydropyridin-3-yl)carbamate 147269-67-8
Price: US $0.00-0.00/g
Min. Order: 1g
Purity: 98%
Supply Ability: 1kg
Release date: 2024-05-21

147269-67-8, BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATERelated Search:

Diethyl 1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate 3-Benzyloxycarbonylamino-6-methyl-2-pyridone BENZYL (5-OXO-1,2,3,5-TETRAHYDROINDOLIZIN-6-YL)CARBAMATE 1-(T-BUTYLOXYCARBONYLMETHYL)-3-(BENZYLOXYCARBONYLAMINO)-2-PYRIDONE BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE

(2-Oxo-1,2-dihydropyridin-3-yl)carbamic acid benzyl ester

benzyl N-(2-oxo-1,2-dihydropyridin-3-yl)carbaMate

benzyl 2-hydroxypyridin-3-ylcarbaMate

BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE

Carbamic acid, N-(1,2-dihydro-2-oxo-3-pyridinyl)-, phenylmethyl ester

BENZYL 2-OXO-1,2-DIHYDROPYRIDIN-3-YLCARBAMATE ISO 9001：2015 REACH

3-(Cbz-amino)pyridin-2(1H)-one

benzyl N-(2-oxo-1H-pyridin-3-yl)carbamate

2-Oxo-1,2-dihydropyridine-3-carbamic acid benzyl ester

147269-67-8