DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE

Product Name
DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE
CAS No.
103588-79-0
Chemical Name
DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE
Synonyms
TDS TRIFLATE;ThexyldimethylsilylTriflate;Dimethyl(1,1,2-trimethylpropyl)silyl triflate;THEXYL-DIMETHYLSILYL TRIFLUOROMETHANSULFONATE;DIMETHYLTHEXYLSILYL TRIFLUOROMETHANESULFONATE;thexyl-dimethylsilyl trifluoromethanesul fonate;TRIFLUOROMETHANESULFONIC AND THEXYL-DIMETHYLSILYL ESTER;DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE;(2,3-Dimethylbutan-2-yl)dimethylsilyl-trifluoromethanesulfonate;Methanesulfonic acid, 1,1,1-trifluoro-, dimethyl(1,1,2-trimethylpropyl)silyl ester
CBNumber
CB7492248
Molecular Formula
C9H19F3O3SSi
Formula Weight
292.39
MOL File
103588-79-0.mol
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DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE Property

Boiling point:
53-54 °C0.6 mm Hg(lit.)
Density 
1.16 g/mL at 20 °C(lit.)
refractive index 
n20/D 1.405
Flash point:
85 °C
solubility 
CH2Cl2, CHCl3, Et2O, THF (can result in ring opening of THF), DMF; reacts with alcohols and water.
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Safety

Hazard Codes 
C
Risk Statements 
14-34
Safety Statements 
26-27-36/37/39-45
RIDADR 
UN 3265 8/PG 2
WGK Germany 
3
10-21
HazardClass 
8
PackingGroup 
III
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
ORS0000840
Product name
DIMETHYLTHEXYLSILYL TRIFLUOROMETHANESULFONATE
Purity
95.00%
Packaging
1G
Price
$231
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
ORS0000840
Product name
DIMETHYLTHEXYLSILYL TRIFLUOROMETHANESULFONATE
Purity
95.00%
Packaging
5ML
Price
$841.88
Updated
2021/12/16
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DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE Chemical Properties,Usage,Production

Physical properties

clear light yellow liquid, bp 40–42 °C/0.15 Torr, 53–54 °C/0.6 mmHg; d = 1.16 g mL?1 at 20 °C; n20 D 1.405.

Uses

Silylation reagent used to introduce the dimethylthexylsilyl (TDS) group; complexation reagent to activate electrophiles. Dimethylthexylsilyl trifluoromethanesulfonate (TDSOTf) is generally used as a bulky silylation reagent.

Preparation

Dimethylthexylsilyl chloride and trifluoromethanesulfonic acid are heated to 60°Cfor 4–5 h and the resulting silyl ester is isolated by distillation.

DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE Preparation Products And Raw materials

Raw materials

Preparation Products

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DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE Suppliers

Nanjing Chemlin Chemical Co., Ltd
Tel
025-83697070
Fax
+86-25-83453306
Email
info@chemlin.com.cn
Country
China
ProdList
19173
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64
Beijing FYF Chemicals Co., Ltd
Tel
010-57903446 15869909019
Fax
010-57903446
Email
168931144@qq.com
Country
China
ProdList
2997
Advantage
58
Shanghai XinKai Chemical Technology Co., Ltd.
Tel
021-58930698 15921516558
Fax
86-021-58933679
Email
zhangyichao84@126.com
Country
China
ProdList
894
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55
Suzhou Siso new material Co.,Ltd.
Tel
0512-65402974 18550909935;
Fax
0512-67544899
Email
siso03@126.com
Country
China
ProdList
1902
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58
Alfa Chemistry
Tel
Fax
1-516-927-0118
Email
Info@alfa-chemistry.com
Country
United States
ProdList
24072
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58
Shanghai Jiegu Biotechnology Co., Ltd.
Tel
021-51698675
Email
jiejiegroup@126.com
Country
China
ProdList
4264
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58
Shanghai Qiming New Material Co. LTD
Tel
021-36010885 13661599081
Fax
021-66167180
Email
sale@qmsilicon.com
Country
China
ProdList
1434
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Beijing InnoChem Science & Technology Co., Ltd.
Tel
15652467323 15652467323
Email
sales@inno-chem.com.cn
Country
China
ProdList
8293
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58
ShenZhen Trendseen Biological Technology Co.,Ltd.
Tel
13417589054 13417589054
Email
trendseenbio@gmail.com
Country
China
ProdList
9470
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58
Shenzhen Nexconn Pharmatechs Ltd
Tel
+86-755-89396905 +86-15013857715
Email
admin@nexconn.com
Country
China
ProdList
10310
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103588-79-0, DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATERelated Search:


  • TDS TRIFLATE
  • THEXYL-DIMETHYLSILYL TRIFLUOROMETHANSULFONATE
  • TRIFLUOROMETHANESULFONIC AND THEXYL-DIMETHYLSILYL ESTER
  • DIMETHYLTHEXYLSILYL TRIFLUOROMETHANESULFONATE
  • DIMETHYL-(2,3-DIMETHYL-2-BUTYL)SILYL TRIFLUOROMETHANESULFONATE
  • thexyl-dimethylsilyl trifluoromethanesul fonate
  • Dimethyl-(2,3-dimethyl-2-butyl)silyl trifluoromethanesulfonate, TDS triflate, Thexyl-dimethylsilyl trifluoromethanesulfonate, Trifluoromethanesulfonic acid thexyl-dimethylsilyl ester
  • (2,3-Dimethylbutan-2-yl)dimethylsilyl-trifluoromethanesulfonate
  • ThexyldimethylsilylTriflate
  • Methanesulfonic acid, 1,1,1-trifluoro-, dimethyl(1,1,2-trimethylpropyl)silyl ester
  • Dimethyl(1,1,2-trimethylpropyl)silyl triflate
  • 103588-79-0
  • C9H19F3O3SSi
  • Protecting and Derivatizing Reagents
  • Protection and Derivatization
  • Silicon-Based
  • Synthetic Reagents