4-(2,2-DIETHOXYETHYL)MORPHOLINE

Product Name: 4-(2,2-DIETHOXYETHYL)MORPHOLINE
CAS No.: 3616-59-9
Chemical Name: 4-(2,2-DIETHOXYETHYL)MORPHOLINE
Synonyms: SKL574;4-(2,2-DIETHOXYETHYL)MORPHOLINE;Morpholine, 4-(2,2-diethoxyethyl)-;2-MORPHOLINOACETALDEHYDE DIETHYLACETAL;4-(2,2-diethoxyethyl)morpholine - [AC78382]
CBNumber: CB7713091
Molecular Formula: C10H21NO3
Formula Weight: 203.28
MOL File: 3616-59-9.mol

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4-(2,2-DIETHOXYETHYL)MORPHOLINE Property

Boiling point:: 80 °C(Press: 0.5 Torr)
Density: 0.990±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 7.16±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H319Causes serious eye irritation
Precautionary statements: P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S767158
Product name: 2-MORPHOLINOACETALDEHYDE DIETHYLACETAL
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $30.7
Updated: 2025/07/31

Sigma-Aldrich

Product number: S767158
Product name: 2-MORPHOLINOACETALDEHYDE DIETHYLACETAL
Purity: AldrichCPR
Packaging: 50MG
Price: $29.8
Updated: 2024/03/01

AK Scientific

Product number: 2438AJ
Product name: 4-(2,2-Diethoxyethyl)morpholine
Packaging: 1g
Price: $104
Updated: 2021/12/16

Matrix Scientific

Product number: 120016
Product name: 4-(2,2-Diethoxyethyl)morpholine
Purity: 95+%
Packaging: 1g
Price: $360
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0024281
Product name: 4-(2,2-DIETHOXYETHYL)MORPHOLINE
Purity: 95.00%
Packaging: 50MG
Price: $727.65
Updated: 2021/12/16

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4-(2,2-DIETHOXYETHYL)MORPHOLINE Chemical Properties,Usage,Production

Synthesis

110-91-8

2032-35-1

3616-59-9

Example 28 - Preparation of Compound 23: The generalized method used for the synthesis of Cmpd 23 analogs is shown in Scheme 2. Scheme 2 involves the process of synthesizing intermediates 7 to 9 and compound 23. Synthesis of intermediate 7: 2-bromoacetaldehyde diethyl acetal (4.5 g, 22.9 mmol), morpholine (2.0 g, 22.9 mmol) and K2CO3 (6.34 g, 45.9 mmol, 2 equiv) were mixed and the reaction was stirred for 16 hours at 120°C. After completion of the reaction, it was cooled to room temperature, diluted with water (50 mL) and extracted with DCM (3 x 50 mL). The organic layers were combined, washed sequentially with saturated aqueous NaHCO3 (50 mL) and brine (50 mL), dried over Na2SO4, filtered and concentrated to give the crude product. The crude product was purified by silica gel column chromatography (100-200 mesh) using 0-50% EtOAc-hexane gradient elution to afford Intermediate 7 (2.6 g, 56%) as a light yellow liquid.1H NMR (CDCl3) δ: 4.64 (t, J=5.3 Hz, 1H), 3.63-3.70 (m, 6H), 3.50-3.58 (m, 2H ), 2.52-2.55 (m, 6H), 1.20 (t, J=7.0Hz, 6H).TLC (hexane solution in 60% EtOAc): Rf=0.50.

References

[1] Patent: WO2011/126903, 2011, A2. Location in patent: Page/Page column 78
[2] Patent: US2017/326125, 2017, A1. Location in patent: Paragraph 0297-0298
[3] Patent: WO2015/131080, 2015, A1. Location in patent: Paragraph 00472; 00473
[4] Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959, vol. 248, p. 2015
[5] Organic and Biomolecular Chemistry, 2011, vol. 9, # 17, p. 5930 - 5933

4-(2,2-DIETHOXYETHYL)MORPHOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(2,2-DIETHOXYETHYL)MORPHOLINE Suppliers

China 44 India 1 United Kingdom 2 United States 8 Global 55

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View Lastest Price from 4-(2,2-DIETHOXYETHYL)MORPHOLINE manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 4-(2,2-DIETHOXYETHYL)MORPHOLINE 3616-59-9
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2025-07-07

Shaanxi Dideu Medichem Co. Ltd

Product: 4-(2,2-DIETHOXYETHYL)MORPHOLINE 3616-59-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20t
Release date: 2024-07-12

3616-59-9, 4-(2,2-DIETHOXYETHYL)MORPHOLINERelated Search:

4-(2,2-DIETHOXYETHYL)MORPHOLINE N-Methyl-bis(2-methoxyethyl)amine BIS(2-METHOXYETHYL)AMINE 2,2-Diethoxy-N,N-dimethylethylamine BIS(2-ETHOXYETHYL)AMINE 2-Morpholinoethanol 2,2-Diethoxyethylamine 2,2-Diethoxytriethylamine (Dimethylamino)acetaldehyde Dimethyl Acetal AKOS 232-06 Methylaminoacetaldehyde dimethyl acetal (2,2-DIETHOXY-ETHYL)-ETHYL-AMINE

4-(2,2-DIETHOXYETHYL)MORPHOLINE

Morpholine, 4-(2,2-diethoxyethyl)-

SKL574

2-MORPHOLINOACETALDEHYDE DIETHYLACETAL

4-(2,2-diethoxyethyl)morpholine - [AC78382]

3616-59-9

pharmacetical