2-IODO-4-METHOXYPHENYLAMINE
- Product Name
- 2-IODO-4-METHOXYPHENYLAMINE
- CAS No.
- 191348-14-8
- Chemical Name
- 2-IODO-4-METHOXYPHENYLAMINE
- Synonyms
- 4-Amino-3-iodoanisole;2-iodo-4-methoxyaniline;4-Methoxy-2-iodoaniline;2-IODO-4-METHOXYPHENYLAMINE;Benzenamine, 2-iodo-4-methoxy-;191348-14-8;4-AMino-3-iodoanisole[2-Iodo-4-Methoxyaniline];2-IODO-4-METHOXYPHENYLAMINE ISO 9001：2015 REACH
- CBNumber
- CB7727764
- Molecular Formula
- C7H8INO
- Formula Weight
- 249.05
- MOL File
- 191348-14-8.mol
2-IODO-4-METHOXYPHENYLAMINE Property
- Boiling point:
- 305.0±27.0 °C(Predicted)
- Density
- 1.807±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 3.14±0.10(Predicted)
- form
- liquid
- color
- Brown to black
Safety
- Hazard Codes
- Xi
- HS Code
- 2921490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I708588
- Product name
- 2-Iodo-4-methoxyaniline
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- I708588
- Product name
- 2-Iodo-4-methoxyaniline
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 079758
- Product name
- 2-Iodo-4-methoxyphenylamine
- Packaging
- 250mg
- Price
- $20
- Updated
- 2021/12/16
- Product number
- 079758
- Product name
- 2-Iodo-4-methoxyphenylamine
- Packaging
- 1g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- W4105
- Product name
- 2-Iodo-4-methoxyphenylamine
- Packaging
- 1g
- Price
- $104
- Updated
- 2021/12/16
2-IODO-4-METHOXYPHENYLAMINE Chemical Properties,Usage,Production
Chemical Properties
Brown liqui
Synthesis
157496-75-8
191348-14-8
The general procedure for the synthesis of 2-iodo-4-methoxyaniline from tert-butyl (2-iodo-4-methoxyphenyl)carbamate was as follows: tert-butyl (2-iodo-4-methoxyphenyl)carbamate (3.5 g, 10.0 mmol) was slowly added to a solution of (2-iodo-4-methoxyphenyl)carbamate in dichloromethane (50 mL) at 0 °C with trifluoroacetic acid (8.9 mL, 120.0 mmol). The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and the reaction was quenched with 2N sodium hydroxide solution (95 mL), followed by adjusting the pH to 8 with 2N hydrochloric acid (70 mL).The organic and aqueous layers were separated, and the aqueous layer was extracted with dichloromethane (2 x 70 mL). All organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by fast column chromatography (silica gel, n-hexane/ethyl acetate = 7:1) to give 2-iodo-4-methoxyaniline (2.12 g, 85% yield) as an orange oil.
References
[1] Organic and Biomolecular Chemistry, 2016, vol. 14, # 6, p. 2127 - 2133
[2] Chemical Communications, 2001, # 24, p. 2732 - 2733
[3] Organic and Biomolecular Chemistry, 2003, vol. 1, # 1, p. 117 - 122
[4] Organometallics, 2013, vol. 32, # 2, p. 682 - 690
[5] Tetrahedron, 2013, vol. 69, # 45, p. 9481 - 9493
2-IODO-4-METHOXYPHENYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-IODO-4-METHOXYPHENYLAMINE manufacturers
- Product
- 2-IODO-4-METHOXYPHENYLAMINE 191348-14-8
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08