ChemicalBook > CAS DataBase List > 2-IODO-4-METHOXYPHENYLAMINE

2-IODO-4-METHOXYPHENYLAMINE

Product Name: 2-IODO-4-METHOXYPHENYLAMINE
CAS No.: 191348-14-8
Chemical Name: 2-IODO-4-METHOXYPHENYLAMINE
Synonyms: 4-Amino-3-iodoanisole;2-iodo-4-methoxyaniline;4-Methoxy-2-iodoaniline;2-IODO-4-METHOXYPHENYLAMINE;Benzenamine, 2-iodo-4-methoxy-;191348-14-8;4-AMino-3-iodoanisole[2-Iodo-4-Methoxyaniline];2-IODO-4-METHOXYPHENYLAMINE ISO 9001：2015 REACH
CBNumber: CB7727764
Molecular Formula: C7H8INO
Formula Weight: 249.05
MOL File: 191348-14-8.mol

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2-IODO-4-METHOXYPHENYLAMINE Property

Boiling point:: 305.0±27.0 °C(Predicted)
Density: 1.807±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 3.14±0.10(Predicted)
form: liquid
color: Brown to black

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Safety

Hazard Codes: Xi
HS Code: 2921490090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: I708588
Product name: 2-Iodo-4-methoxyaniline
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: I708588
Product name: 2-Iodo-4-methoxyaniline
Packaging: 500mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: W4105
Product name: 2-Iodo-4-methoxyphenylamine
Packaging: 1g
Price: $104
Updated: 2021/12/16

Apolloscientific

Product number: OR400551
Product name: 2-Iodo-4-methoxyaniline
Packaging: 1g
Price: $114
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4656-H-11
Product name: 2-Iodo-4-methoxyaniline
Packaging: 1g
Price: $125
Updated: 2021/12/16

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2-IODO-4-METHOXYPHENYLAMINE Chemical Properties,Usage,Production

Chemical Properties

Brown liqui

Synthesis

157496-75-8

191348-14-8

The general procedure for the synthesis of 2-iodo-4-methoxyaniline from tert-butyl (2-iodo-4-methoxyphenyl)carbamate was as follows: tert-butyl (2-iodo-4-methoxyphenyl)carbamate (3.5 g, 10.0 mmol) was slowly added to a solution of (2-iodo-4-methoxyphenyl)carbamate in dichloromethane (50 mL) at 0 °C with trifluoroacetic acid (8.9 mL, 120.0 mmol). The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and the reaction was quenched with 2N sodium hydroxide solution (95 mL), followed by adjusting the pH to 8 with 2N hydrochloric acid (70 mL).The organic and aqueous layers were separated, and the aqueous layer was extracted with dichloromethane (2 x 70 mL). All organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by fast column chromatography (silica gel, n-hexane/ethyl acetate = 7:1) to give 2-iodo-4-methoxyaniline (2.12 g, 85% yield) as an orange oil.

References

[1] Organic and Biomolecular Chemistry, 2016, vol. 14, # 6, p. 2127 - 2133
[2] Chemical Communications, 2001, # 24, p. 2732 - 2733
[3] Organic and Biomolecular Chemistry, 2003, vol. 1, # 1, p. 117 - 122
[4] Organometallics, 2013, vol. 32, # 2, p. 682 - 690
[5] Tetrahedron, 2013, vol. 69, # 45, p. 9481 - 9493

2-IODO-4-METHOXYPHENYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-IODO-4-METHOXYPHENYLAMINE manufacturers

Career Henan Chemical Co

Product: 2-IODO-4-METHOXYPHENYLAMINE 191348-14-8
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

191348-14-8, 2-IODO-4-METHOXYPHENYLAMINERelated Search:

3-Iodoanisole 3-IODO-4-NITROANISOLE 2-IODO-4-TRIFLUOROMETHOXYANILINE N-BOC-4-ETHOXY-2-IODOPHENYLAMINE 5-IODO-6-AMINO-1,2-BENZOPYRONE 2-IODO-4-METHOXYPHENYLAMINE 2-BROMO-6-IODO-4-TRIFLUOROMETHOXYANILINE BUTTPARK 83\07-25 2,2-DIFLUORO-5-AMINO-6-IODO-1,3-BENZODIOXOLE 5-IODO-6-NITRO-1,3-BENZODIOXOLE 4-ETHOXY-2-IODOPHENYLAMINE tert-Butyl 2-iodo-4-methoxyphenylcarbamate

4-AMino-3-iodoanisole[2-Iodo-4-Methoxyaniline]

4-Methoxy-2-iodoaniline

2-iodo-4-methoxyaniline

4-Amino-3-iodoanisole

2-IODO-4-METHOXYPHENYLAMINE

Benzenamine, 2-iodo-4-methoxy-

2-IODO-4-METHOXYPHENYLAMINE ISO 9001：2015 REACH

191348-14-8

1191348-14-8

pharmacetical