6-Methoxy-2-methylpyridin-3-amine
- Product Name
- 6-Methoxy-2-methylpyridin-3-amine
- CAS No.
- 52090-56-9
- Chemical Name
- 6-Methoxy-2-methylpyridin-3-amine
- Synonyms
- 5-AMINO-2-METHOXY-6-PICOLINE;3-AMINO-6-METHOXY-2-PICOLINE;6-Methoxy-2-methyl-3-pyridinamine;3-Pyridinamine,6-methoxy-2-methyl;2-Methyl-6-methoxypyridin-3-amine;6-Methoxy-2-methyl-3-pyridylamine;6-methoxy-2-methylpyridin-3-amine;2-Methyl-3-amine-6-methoxypyridine;2-Methoxy-5-amino-6-methylpyridine;6-Methoxy-2-methyl-pyridin-3-ylamine
- CBNumber
- CB7740231
- Molecular Formula
- C7H10N2O
- Formula Weight
- 138.17
- MOL File
- 52090-56-9.mol
6-Methoxy-2-methylpyridin-3-amine Property
- Boiling point:
- 260.0±35.0 °C(Predicted)
- Density
- 1.103±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 5.05±0.10(Predicted)
- Appearance
- Light yellow to brown Solid-Liquid Mixture
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M218888
- Product name
- 6-Methoxy-2-methylpyridin-3-amine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- X3021
- Product name
- 3-Amino-6-methoxy-2-methylpyridine
- Packaging
- 1g
- Price
- $63
- Updated
- 2021/12/16
- Product number
- FA55483
- Product name
- 3-Amino-6-methoxy-2-methylpyridine
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- OR345360
- Product name
- 3-Amino-6-methoxy-2-methylpyridine
- Purity
- 98%
- Packaging
- 5g
- Price
- $192
- Updated
- 2021/12/16
- Product number
- 4H56-1-613
- Product name
- 3-Amino-6-methoxy-2-methylpyridine
- Purity
- 98%
- Packaging
- 5G
- Price
- $212
- Updated
- 2021/12/16
6-Methoxy-2-methylpyridin-3-amine Chemical Properties,Usage,Production
Synthesis
5467-69-6
52090-56-9
6-Methoxy-2-methyl-3-nitropyridine (2 g, 0.012 mol) was used as starting material, which was dissolved in H2O/MeOH (1:1, 40 mL) mixed solvent. Subsequently, NH4Cl (2.2 g, 3.5 eq.) and iron powder (2.3 g, 3.5 eq.) were added to the solution. The reaction mixture was stirred at 80 °C for 16 hours. After completion of the reaction, the iron powder was removed by filtration and the filtrate was washed with MeOH. The MeOH was removed from the filtrate by evaporation, diluted with H2O, and then the aqueous phase was extracted with EtOAc (3 x 50 mL). The organic phases were combined and dried with anhydrous Na2SO4. The desiccant was removed by filtration and the solvent was evaporated to dryness to give 2-methoxy-5-amino-6-methylpyridine (1.35 g, 81% yield) as a brown oil. Its nuclear magnetic resonance hydrogen spectrum (1H NMR, CDCl3) data were as follows: δ 6.9 (d, 1H), 6.4 (d, 1H), 3.8 (s, 3H), 2.33 (s, 3H).
References
[1] Patent: WO2004/62665, 2004, A1. Location in patent: Page/Page column 45
[2] Journal of the Chemical Society, <1954> 2448, 2452,
6-Methoxy-2-methylpyridin-3-amine Preparation Products And Raw materials
Raw materials
Preparation Products
6-Methoxy-2-methylpyridin-3-amine Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 6-Methoxy-2-methylpyridin-3-amine manufacturers
- Product
- 3-AMINO-6-METHOXY-2-PICOLINE 52090-56-9
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-06
- Product
- 3-AMINO-6-METHOXY-2-PICOLINE 52090-56-9
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2019-12-26