2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE

Product Name: 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE
CAS No.: 50432-67-2
Chemical Name: 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE
Synonyms: 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE;3,4-Pyridinediamine, 2-chloro-N4-methyl-;2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE ISO 9001：2015 REACH
CBNumber: CB7795266
Molecular Formula: C6H8ClN3
Formula Weight: 157.6
MOL File: 50432-67-2.mol

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2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: Brown to dark brown Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C611198
Product name: 2-Chloro-N4-methylpyridine-3,4-diamine
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC147667
Product name: 2-Chloro-n4-methylpyridine-3,4-diamine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC147667
Product name: 2-Chloro-n4-methylpyridine-3,4-diamine
Packaging: 250mg
Price: $120
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC147667
Product name: 2-Chloro-n4-methylpyridine-3,4-diamine
Packaging: 500mg
Price: $210
Updated: 2021/12/16

Matrix Scientific

Product number: 072557
Product name: 2-Chloro-N4-methylpyridine-3,4-diamine
Purity: 95+%
Packaging: 250mg
Price: $231
Updated: 2021/12/16

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2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE Chemical Properties,Usage,Production

Synthesis

1633-41-6

50432-67-2

General procedure for the synthesis of 2-chloro-N4-methylpyridine-3,4-diamine from 4-methylamino-3-nitropyridine: 0.61 g (4.0 mmol) of 4-methylamino-3-nitropyridine was dissolved in 3.5 mL of concentrated hydrochloric acid. The reaction mixture was heated to 90 °C. Subsequently, a suspension of 3.5 g (15 mmol) of stannous chloride in concentrated hydrochloric acid (4 mL) was slowly added. The reaction mixture was reacted under reflux conditions for 3 hours. Upon completion of the reaction, the suspension was cooled to room temperature, poured into 75 mL of water and extracted with dichloromethane (2 x 30 mL). The organic layers were combined, dried with magnesium sulfate and concentrated in vacuum to give 0.60 g (95% yield) of 2-chloro-N4-methylpyridine-3,4-diamine as a white solid with a melting point of 168-169 °C.

References

[1] Patent: WO2005/26164, 2005, A1. Location in patent: Page/Page column 42
[2] Journal of Medicinal Chemistry, 2005, vol. 48, # 22, p. 6887 - 6896
[3] Patent: EP1568699, 2005, A1. Location in patent: Page/Page column 82

2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE manufacturers

Dideu Industries Group Limited

Product: 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE 50432-67-2
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-07

50432-67-2, 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINERelated Search:

4-Amino-5-chloro-N-(2-(diethylamino)ethyl)-2-methoxybenzamide 2-CHLORO-N,6-DIMETHYL-3-NITROPYRIDIN-4-AMINE 2-chloro-N4-ethylpyridine-3,4-diamine 2-CHLORO-N4,6-DIMETHYLPYRIDINE-3,4-DIAMINE (2-CHLORO-3-NITRO-QUINOLIN-4-YL)-ISOBUTYL-AMINE 2-Chloro-N4-(2-methypropyl)-3,4-quinolinediamine 2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE 4-Pyridinamine,2-chloro-5,6-dimethyl-3-nitro-N-(phenylmethyl)- 2-CHLORO-N,N,6-TRIMETHYL-3-NITROPYRIDIN-4-AMINE 2-chloro-N4-(1-methylethyl)pyridine-3,4-diamine

2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE

3,4-Pyridinediamine, 2-chloro-N4-methyl-

2-CHLORO-N4-METHYLPYRIDINE-3,4-DIAMINE ISO 9001：2015 REACH

50432-67-2

Heterocycle-Pyridine series

pharmacetical