3-METHOXY-4-NITROBENZALDEHYDE

Product Name: 3-METHOXY-4-NITROBENZALDEHYDE
CAS No.: 80410-57-7
Chemical Name: 3-METHOXY-4-NITROBENZALDEHYDE
Synonyms: 3-METHOXY-4-NITROBENZALDEHYDE;Benzaldehyde, 3-Methoxy-4-nitro-;3-Methoxy-4-nitrobenzaldehyde 97%
CBNumber: CB7829893
Molecular Formula: C8H7NO4
Formula Weight: 181.15
MOL File: 80410-57-7.mol

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3-METHOXY-4-NITROBENZALDEHYDE Property

Melting point:: 104 °C
Boiling point:: 354.7±27.0 °C(Predicted)
Density: 1.322±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: crystalline powder
color: Cream/gold/faint tan

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Safety

HS Code: 2912290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M266588
Product name: 3-methoxy-4-nitrobenzaldehyde
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: OR400210
Product name: 3-Methoxy-4-nitrobenzaldehyde
Purity: 97%
Packaging: 1g
Price: $127
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-1-4M
Product name: 3-Methoxy-4-nitrobenzaldehyde
Purity: 97%
Packaging: 1g
Price: $140
Updated: 2021/12/16

Apolloscientific

Product number: OR400210
Product name: 3-Methoxy-4-nitrobenzaldehyde
Purity: 97%
Packaging: 5g
Price: $414
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-1-4M
Product name: 3-Methoxy-4-nitrobenzaldehyde
Purity: 97%
Packaging: 5G
Price: $456
Updated: 2021/12/16

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3-METHOXY-4-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

704-13-2

74-88-4

80410-57-7

(1) Synthesis of 3-methoxy-4-nitrobenzaldehyde: 3-hydroxy-4-nitrobenzaldehyde (500 mg, 2.99 mmol) and potassium carbonate (0.42 g, 3.0 mmol) were dissolved in 6.0 mL of N,N-dimethylformamide. Iodomethane (0.38 mL, 6.0 mmol) was slowly added to the reaction system at room temperature, followed by continuous stirring at the same temperature for 5 hours. After completion of the reaction, the reaction mixture was diluted with ethyl acetate and water and separated. The organic layer was washed twice with saturated brine and subsequently dried with anhydrous magnesium sulfate. After filtration, the filtrate was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate = 4/1 to 1/1) to afford the target compound, 3-methoxy-4-nitrobenzaldehyde, as a light yellow powder (518 mg, 96% yield).

References

[1] ACS Medicinal Chemistry Letters, 2017, vol. 8, # 10, p. 1002 - 1006
[2] Patent: WO2016/124747, 2016, A1. Location in patent: Page/Page column 62; 63
[3] Patent: US2018/202388, 2018, A1
[4] Patent: EP2123637, 2009, A1. Location in patent: Page/Page column 19
[5] Organic and Biomolecular Chemistry, 2014, vol. 12, # 30, p. 5629 - 5633

3-METHOXY-4-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-METHOXY-4-NITROBENZALDEHYDE Suppliers

China 26 India 4 United Kingdom 1 United States 6 Global 37

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80410-57-7, 3-METHOXY-4-NITROBENZALDEHYDERelated Search:

3-Methoxy-4-nitrobenzoic acid Methyl 3-methoxy-4-nitrobenzoate 2-Amino-4-nitro-5-methoxybenzoic Acid Methyl 3-(2-ethoxy-2-oxoethoxy)-4-nitrobenzoate 3-BUTOXY-4-NITROBENZOIC ACID 3-METHOXY-4-NITROBENZALDEHYDE 6,7-Dibromo-8-nitro-2,3-dihydrobenzo[1,4]dioxine-5-carboxylic acid 3-METHOXY-4-NITROACETOPHENONE 1-(6,7-DICHLORO-8-NITRO-2,3-DIHYDRO-1,4-BENZODIOXIN-5-YL)-1-ETHANONE TERT-BUTYL 3-METHOXY-4-NITROBENZOATE METHYL 3-[(2-FLUOROBENZOYL)OXY]-4-NITROBENZENECARBOXYLATE 3-[(5-FORMYL-2-METHOXYBENZYL)OXY]-4-NITROBENZOIC ACID 5-(METHOXYCARBONYL)-2-NITROPHENYL 2-THIOPHENECARBOXYLATE 2,5-Diethoxy-4-Nitro-Benzanilide METHYL 3-[(4-METHYLBENZOYL)OXY]-4-NITROBENZENECARBOXYLATE ethyl 2,5-dimethoxy-4-nitrobenzoate 3,5-DIMETHOXY-4-NITROBENZOIC ACID 2,5-dimethoxy-4-nitrobenzoic acid

3-METHOXY-4-NITROBENZALDEHYDE

Benzaldehyde, 3-Methoxy-4-nitro-

3-Methoxy-4-nitrobenzaldehyde 97%

80410-57-7